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Table of contents
- Contentsv
- Prefacevii
- Chapter 1. The Theoretical and Practical Limits of Resolution in Multiple-Pulse High-Resolution NMR1
- I. Introduction1
- II. Computer Simulations of Multiple-Pulse Experiments6
- III. Multiple-Pulse Spectrometer26
- IV. Experimental Tests of Simulations: Practical Limits of Resolution41
- V. Ab Initio Calculation of Proton Shielding Tensors: Comparison with Experiments52
- References56
- Chapter 2. Homonuclear and Heteronuclear Hartmann–Hahn Transfer in Isotropic Liquids59
- I. Introduction60
- II. Principle of Hartmann–Hahn Transfer63
- III. Multiple-Pulse Sequences74
- IV. Theoretical Tools79
- V. Classification of Hartmann–Hahn Experiments97
- VI. Hartmann–Hahn Transfer in Multispin Systems113
- VII. Symmetry and Hartmann–Hahn Transfer134
- VIII. Development of Hartmann–Hahn Mixing Sequences139
- IX. Assessment of Multiple–Pulse Sequences144
- X. Homonuclear Hartmann–Hahn Sequences158
- XI. Heteronuclear Hartmann–Hahn Sequences196
- XII. Practical Aspects of Hartmann–Hahn Experiments209
- XIII. Combinations and Applications221
- XIV. Conclusion238
- List of Abbreviations239
- References241
- Chapter 3. Millimeter Wave Electron Spin Resonance Using Quasioptical Techniques253
- I. Introduction253
- II. Components260
- III. Mathematical Background264
- IV. Quasioptical Beam Guides274
- V. Design Criteria for Beam Guides277
- VI. Fabry–Pérot Resonators280
- VII. Transmission Mode Resonator287
- VIII. Spectrometer Sensitivity290
- IX. Reflection Mode Spectrometer296
- X. An Adjustable Finesse Fabry–Pérot Resonator306
- XI. Optimization of Resonators314
- XII. Summary316
- Appendix: Higher Order Gaussian Beam Modes317
- References321
- Chapter 4. Generalized Analysis of Motion Using Magnetic Field Gradients325
- I. Introduction326
- II. Generalized Motion327
- III. Modulated Gradient Spin-Echo NMR330
- IV. Self-Diffusion in Restricted Geometries351
- V. PGSE and Multidimensional NMR361
- VI. Self-Diffusion with a Strong Inhomogeneous Magnetic Field371
- VII. Migration in an Inhomogeneous rf Field380
- VIII. Conclusions382
- Appendix383
- References385
- Index389
Book details
- Vendor Elsevier S & T
- SKU 9780120255191
- ISBN-13 9780080526300
- Author Warren, Warren S.
- Category Science
- Subject Analytic
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Since 1965, Advances in Magnetic and Optical Resonance has provided researchers with timely expositions of fundamental new developments in the theory of, experimentation with, and application of magnetic and optical resonance.
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