Elsevier S & T

Annual Reports on NMR Spectroscopy

Webb, Graham A.

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Table of contents
  • Contentsv
  • Contributorsvii
  • Prefaceix
  • 1. Structure and Membrane Interactions of Antimicrobial Peptides as Viewed by Solid-State NMR Spectr1
  • 1. Introduction2
  • 2. Study of Antimicrobial Peptides in Membranes3
  • 3. Effects of Antimicrobial Peptides on Model Lipid Membranes15
  • 4. Conclusions19
  • References19
  • 2. Chemical Exchange23
  • 1. Introduction23
  • 2. Overview, Trends and Opinions25
  • 3. Theory27
  • 4. Methodology32
  • 5. Applications35
  • 6. Conclusions and Acknowledgments43
  • References44
  • 3. Rhodium-103 NMR49
  • 1. Introduction50
  • 2. Acquisition of Data51
  • 3. Calibration of Spectra52
  • 4. Factors Underlying the Chemical Shift54
  • 5. Influence of Temperature on the Chemical Shift57
  • 6. Influence of Solvent on the Chemical Shift58
  • 7. Other Influences on the Chemical Shift61
  • 8. Correlation of δ(103Rh) with Chemical and Structural Parameters65
  • 9. Parahydrogen-Induced Polarisation (PHIP)76
  • 10. High-Pressure Studies78
  • 11. Solid-State Studies78
  • 12. Clusters80
  • 13. Calculated Chemical Shifts82
  • 14. Spin Coupling Constants84
  • 15. Relaxation Times87
  • 16. Conclusion88
  • Abbreviations88
  • Acknowledgements90
  • Appendix: Layout of Tables90
  • References167
  • 4. The Indirect Detection of Metal Nuclei by Correlation Spectroscopy (HSQC and HMQC)179
  • 1. Introduction180
  • 2. 2D NMR Spectroscopy186
  • 3. Spin Systems200
  • 4. Review of Recent Reports of the Indirect Detection of Metal Nuclei211
  • 5. Conclusions255
  • Abbreviations255
  • Acknowledgements257
  • References257
  • Subject Index263
Book details
  • Vendor Elsevier S & T
  • SKU 9780123742940
  • ISBN-13 9780080560922
  • Author Webb, Graham A.
  • Category Science
  • Subject Spectroscopy & Spectrum Analysis

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Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicists to study the structure and dynamics of molecules. In recent years, no other technique has grown to such importance as NMR spectroscopy. It is used in all branches of science when precise structural determination is required and when the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a premier means for the specialist and non-specialist alike to become familiar with new techniques and applications of NMR spectroscopy.

* Provides updates on the latest developments in NMR spectroscopy
* Includes comprehensive review articles
* Highlights the increasing importance of NMR spectroscopy as a technique for structural determination