Elsevier S & T

Annual Reports on NMR Spectroscopy

Webb, Graham A.

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Table of contents
  • Cover
  • Contentsix
  • List of Contributorsv
  • Prefacevii
  • Chapter 1. A Study of Conformational Stability of Polypeptide Blends by Solid State NMR Spectroscopy1
  • 1. Introduction2
  • 2. Polypeptide blend preparations8
  • 3. 13C CP/MAS NMR spectral analysis and conformational characterization of homopolypeptides and thei10
  • 4. 1HT1pS of homopolypeptides and their blend compatibility27
  • 5. Two-dimensional 13C–1H Hetcor spectral analysis and structural characterization of polypeptides39
  • 6. Conclusions54
  • References54
  • Chapter 2. Applications of Heteronuclear X/Y-Correlation Spectroscopy in Organometallic and Organoel59
  • 1. Introduction60
  • 2. Methods62
  • 3. Recent applications of X/Y correlations87
  • 4. Conclusions99
  • References100
  • Chapter 3. NMR Studies of Biomolecular Dynamics and Structural Plasticity Using Residual Dipolar Cou105
  • 1. Introduction106
  • 2. Theoretical background109
  • 3. Molecular alignment123
  • 4. Applications to protein domains134
  • 5. Protein dynamics at the local level141
  • 6. Applications to RNA152
  • 7. Applications to oligosaccharides157
  • 8. Conclusions and future perspectives159
  • Acknowledgements160
  • References161
  • Chapter 4. Advances in Theoretical and Physical Aspects of Spin–Spin Coupling Constants167
  • 1. Introduction168
  • 2. Calculation and analysis of spin–spin coupling constants171
  • 3. Coupling mechanisms and factors affecting them184
  • Acknowledgements248
  • References248
  • Chapter 5. High Resolution Magic Angle Spinning – Applications to Solid Phase Synthetic Systems an261
  • 1. Introduction261
  • 2. Nature of the samples263
  • 3. Specialized NMR techniques268
  • 4. Applications to polymer-supported species272
  • 5. Applications to polymers, whole cells and tissues279
  • 6. Summary and prospects286
  • References287
  • Index297
Book details
  • Vendor Elsevier S & T
  • SKU 9780125054515
  • ISBN-13 9780080544106
  • Author Webb, Graham A.
  • Category Science
  • Subject Spectroscopy & Spectrum Analysis

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Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicians to study the structure and dynamics of molecules. In recent years, no other technique has grown to such importance as NMR spectroscopy. It is used in all branches of science where precise structural determination is required and where the nature of interactions and reactions in solution is being studied.

Annual Reports on NMR has established itself as a premier means for the specialist and nonspecialist alike to become familiar with new techniques and applications of NMR spectroscopy.

- Includes comprehensive review articles on NMR Spectroscopy
- NMR is used in all branches of science
- No other technique has grown to such importance as NMR Spectroscopy in recent years