Characterisation of Porous Solids V
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Table of contents
- Cover
- Contentsv
- Forewordxiii
- Scientific Committeexv
- Financial Supportxv
- Part I: Theory, Modelling and Simulation1
- Chapter 1. Adsorption of Argon and Xenon in Silica Controlled Porous Glass: A Grand Canonical Monte-1
- Chapter 2. The role of isosteric enthalpy of adsorption in micropore characterisation: A simulation11
- Chapter 3. Capillary Condensation and Hysteresis in Disordered Porous Materials21
- Chapter 4. Molecular Simulation Study on Freezing in Nano-pores31
- Chapter 5. Characterisation of porous materials using density functional theory and molecular simula41
- Chapter 6. Density Functional Theory of Adsorption Hysteresis and Nanopore Characterization51
- Chapter 7. Characterization of controlled pore glasses: Molecular simulations of adsorption61
- Chapter 8. A new method for the accurate pore size analysis of MCM-41 and other silica based mesopor71
- Chapter 9. Comparison of the experimental isosteric heat of adsorption of argon on mesoporous silica81
- Chapter 10. A computational exploration of cation locations in high-silica Ca-Chabazite89
- Chapter 11. Density functional theory: Diatomic nitrogen molecules in graphite pores99
- Chapter 12. Modelling studies of the influence of macroscopic structural heterogeneities on nitrogen111
- Chapter 13. Condensation-evaporation processes in simulated heterogeneous three-dimensional porous n121
- Chapter 14. Characterisation of porous solids for gas transport131
- Chapter 15. Experimental and simulation studies of melting and freezing in porous glasses141
- Chapter 16. A fast two-point method for gas adsorption measurements151
- Part II: Highly Ordered Porous Inorganic Systems155
- Chapter 17. Rational design, tailored synthesis and characterisation of ordered mesoporous silicas i155
- Chapter 18. Relationship between intrinsic pore-wall corrugation and adsorption hysteresis of N2, O2167
- Chapter 19. Study of the morphology of porous silica materials177
- Chapter 20. Adsorption hysteresis and criticality in regular mesoporous materials187
- Chapter 21. Comprehensive structural characterisation of MCM-41: From mesopores to particles197
- Chapter 22. Characterisation of mesoporous MCM-41 adsorbents by various techniques207
- Chapter 23. Characterisation of mesoporous molecular sieves containing copper and zinc: An adsorptio215
- Chapter 24. On the applicability of the Horwath-Kawazoe method for pore size analysis of MCM-41 and225
- Chapter 25. Dynamic and structural properties of confined phases (hydrogen, methane and water) in MC235
- Chapter 26. Estimating pore size distribution from the differential curves of comparison plots243
- Chapter 27. Rotational state change of acetonitrile vapor on MCM-41 upon capillary condensation with251
- Chapter 28. Systematic sorption studies on surface and pore size characteristics of different MCM-48259
- Chapter 29. Synthesis and characterisation of ordered mesoporous MCM-41 materials269
- Chapter 30. Textural and spectroscopic characterisation of vanadium MCM-41 materials - Application t279
- Chapter 31. On the ordering of simple gas phases adsorbed within model microporous adsorbents289
- Chapter 32. Textural and framework-confined porosity in S+I– mesoporous silica297
- Part III: Carbons303
- Chapter 33. Use of immersion calorimetry to evaluate the separation ability of carbon molecular siev303
- Chapter 34. Molecular simulations and measurement of adsorption in porous carbon nanotubes313
- Chapter 35. Application of the alpha s method for analysing benzene, dichloromethane and methanol is323
- Chapter 36. Characterisation of porous carbonaceous sorbents using high pressure - high temperature333
- Chapter 37. Influence of the porous structure of activated carbon on adsorption from binary liquid m347
- Chapter 38. Adsorption mechanism of water on carbon micropore with in situ small angle x-ray scatter355
- Chapter 39. Ultra-thin microporous carbon films361
- Chapter 40. Electrochemical investigation of carbon aerogels and their activated derivatives371
- Chapter 41. Evolution of microporosity upon CO2-activation of carbon aerogels381
- Chapter 42. On the determination of the micropore size distribution of activated carbons from adsorp391
- Chapter 43. Role of pore size distribution in the binary adsorption kinetics of gases in activated c401
- Chapter 44. Confined state of alcohol in carbon micropores as revealed by in situ x-ray diffraction411
- Part IV: Interpretation of Data, Membranes421
- Chapter 45. Critical appraisal of the use of nitrogen adsorption for the characterisation of porous421
- Chapter 46. Structural characterisation and applications of ceramic membranes for gas separations429
- Chapter 47. SANS charcterisation of mesoporous silicas having model structures439
- Chapter 48. Pore-scale complexity of a calcareous material by time-controlled mercury porosimetry449
- Chapter 49. SANS analysis of anisotropic pore structures in alumina membranes459
- Chapter 50. Zeolite membranes - charcterisation and applications in gas separations467
- Chapter 51. A modified Horvath-Kawazoe method for micropore size analysis475
- Part V: Miscellaneous techniques485
- Chapter 52. Further evidences of the usefullness of CO2 adsorption to characterise microporous solid485
- Chapter 53. Interaction between menisci in adjacent pores495
- Chapter 54. Studies on the formation and properties of some highly ordered mesoporous solids505
- Chapter 55. Pore structure of zeolites of type Y and pentasil as the function conditions of preparat515
- Chapter 56. Characterisation of activated carbon fibers by positron annihilation life- time spectros523
- Chapter 57. Investigation of the textural characteristics and their impact on in vitro dissolution o533
- Chapter 58. The response function method as a novel technique to determine the dielectric permittivi545
- Chapter 59. Mesopore characterisation by positron annihilation557
- Chapter 60. Characterisation of vanadia-doped silica aerogeis565
- Chapter 61. Shear strength of mineral filter cakes573
- Chapter 62. A frequency-response study of diffusion and adsorption of C1-C5 alkanes and acetylene in587
- Chapter 63. Novel Mn-based mesoporous mixed oxidic solids593
- Chapter 64. Mercury porosimetry applied to precipitated silica603
- Chapter 65. Synthesis and textural properties of amorphous silica-aluminas613
- Chapter 66. Porous texture modifications of a series of silica and silica-alumina hydrogels and xero623
- Chapter 67. Comparison of specific surface areas of a micronised drug substance as determined by dif633
- Chapter 68. Investigations on the surface properties of pure and alkali or alkaline earth metal dope643
- Chapter 69. Comparison of the porosity evaluation results based on immersion calorimetry and gravime653
- Chapter 70. Measuring permeability and modulus of aerogels using dynamic pressurisation in an autocl663
- Author Index671
- Other volumes in the series675
The Fifth International Symposium on the Characterisation of Porous Solids (COPS-V) was held at Heidelberg, Germany, from May 30 to June 2, 1999. About 220 participants from 25 countries enjoyed a very successful meeting with 32 lectures and 155 poster presentations.
The Symposium started with a highly stimulating lecture by Sir John Meurig Thomas, Cambridge, highlighting the recent developments in engineering of new catalysts. The following two full sessions were devoted to theory, modelling and simulation which provide the basis for the interpretation of pore structural data of adsorbents and finely dispersed solids. Sessions 2 and 3 focused on the advances in the synthesis and characterisation of highly ordered inorganic adsorbents and carbons. Sessions 4 and 5 addressed important questions with respect to the characterisation of porous solids by sorption measurement and other related techniques.
The intensive three-day programme provided a stimulating forum for the exchange of novel research findings, concepts, techniques and materials which are collected in this volume.
The Symposium started with a highly stimulating lecture by Sir John Meurig Thomas, Cambridge, highlighting the recent developments in engineering of new catalysts. The following two full sessions were devoted to theory, modelling and simulation which provide the basis for the interpretation of pore structural data of adsorbents and finely dispersed solids. Sessions 2 and 3 focused on the advances in the synthesis and characterisation of highly ordered inorganic adsorbents and carbons. Sessions 4 and 5 addressed important questions with respect to the characterisation of porous solids by sorption measurement and other related techniques.
The intensive three-day programme provided a stimulating forum for the exchange of novel research findings, concepts, techniques and materials which are collected in this volume.