Elsevier S & T

Characterization of Porous Solids VI: Proceedings of the 6th International Symposium on the Characterization of Porous Solids (COPS-VI), Allicante, Spain, May 8 - 11 2002

Rodríguez-Reinoso, F.

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Table of contents

Cover
Contentsv
Prefacexv
Committeesxvii
Financial supportxvii
Chapter 1. Scanning probe microscopies for the characterization of porous solids: strengths and limi1
Chapter 2. Role of gas adsorption in nanopore characterization11
Chapter 3. Reconstruction method for the characterization of porous carbons19
Chapter 4. A new method for microporosity detection based on the use of the corrugated pore structur27
Chapter 5. Physisorption in nanopores of various sizes and shapes: a Grand Canonical Monte Carlo sim35
Chapter 6. Induced porosity in cross-linked polymer networks: Mean field theory and simulations43
Chapter 7. Microbean small angle X-ray scattering (μSAXS): a novel technique for the characterizati51
Chapter 8. "Real time" determination of porosity development in carbons: a combined SAXS/TGA approac59
Chapter 9. SANS investigations of adsorption mechanisms in model porous silicas67
Chapter 10. Preparation and surface characterization of novel ceria-copper and ceria-manganese mixed75
Chapter 11. About the exclusive mesoporous character of MCM-4183
Chapter 12. Incorporation of appropriate contact angles in textural characterization by mercury poro91
Chapter 13. A two-stage Horvath-Kawazoe adsorption model for pore size distribution analysis99
Chapter 14. Textural and chemical characterization of NaX zeolite exchanged with Zn(ll) ions107
Chapter 15. Evaluation and comparison of the pore structure and related properties of particulate an115
Chapter 16. Percolation phenomena in micropores: influence on single and multicomponent adsorption e123
Chapter 17. Characterization of the surface chemistry of activated carbon by molecular simulation of131
Chapter 18. Comparison of porous carbons developed via templating approaches139
Chapter 19. Simulation of adsorption in 3-D reconstructed mesoporous materials by a simulated anneal147
Chapter 20. Understanding adsorption hysteresis in porous glasses and other mesoporous materials155
Chapter 21. Structural studies of mesoporous alumina membranes by small angle X-ray scattering163
Chapter 22. Assessing microporosity by immersion microcalorimetry into liquid nitrogen or liquid arg171
Chapter 23. The lower closure point of the adsorption hysteresis loop of fluids in mesoporous silica177
Chapter 24. New metodologies in mercury porosimetry185
Chapter 25. Theoretical calculation of high micropore volumes on activated carbons193
Chapter 26. Assessment of ultramicroporosity on carbon molecular sieves by water adsorption201
Chapter 27. Active surface area of carbon materials determined by different methods209
Chapter 28. Heterogeneity of sewage sludge derived materials as a factor governing their performance217
Chapter 29. Evaluation of microporous structure of carbon molecular sieves using the pycnometric met225
Chapter 30. Characterization of porous carbonaceous sorbents using adsorption data in wide temperatu231
Chapter 31. Ammonia accessibility to the porosity of several activated carbons measured by flow adso239
Chapter 32. An IGC and TA study of acetaldehyde adsorption on activated carbons247
Chapter 33. A novel approach for characterizing carbon catalysts by TAP experiments255
Chapter 34. Preparation of activated carbons with controlled pore size261
Chapter 35. Characterization of porous solids using low pressure VOC adsorption data267
Chapter 36. Energetics and mechanism of physical sorption by carbonaceous solids: Evaluation of surf275
Chapter 37. Phenanthrene adsorption on a carbonaceous material: moisture and CO2 influence283
Chapter 38. Water adsorption on micro and mesoporous silicas291
Chapter 39. The effect of surface functionalization of mesoporous silicas with propylimidazol on por299
Chapter 40. Preparation of porous silica by acid activation of metakaolins307
Chapter 41.The effect of particle shape on the filtration rate and shear strength quartz and dolomit315
Chapter 42. Characterisation of silica low-density xerogels in presence of additives by image analys323
Chapter 43. Texture characterization of ultramacroporous materials using non-destructive methods331
Chapter 44. Formation of hierarchically ordered silicas prepared by spray drying of nanosized sphere339
Chapter 45. Ultrathin porous glass membranes with controlled texture properties347
Chapter 46. Reconstruction of mesoporous silica glass Gelsil® 50355
Chapter 47. Pore structural characteristics of mesostructured materials prepared under different con363
Chapter 48. A grand canonical Monte Carlo simulation study of water adsorption in a Vycor-like disor371
Chapter 49. A review of the application of the BET equation to experimental data: the C parameter379
Chapter 50. Thermogravimetric and sorption measurement techniques/instruments387
Chapter 51. Influence of method of washcoat preparation on hydrothermal stability of alumina support395
Chapter 52. Limestone influence on PAH emissions from coal AFBC. Catalytic or/and adsorption effect?403
Chapter 53. Freezing point elevation in nanospace detected directly by atomic force microscopy411
Chapter 54. Is it possible to obtain a coherent image of the texture of a porous material?419
Chapter 55. Preparation and characterisation of Cr-Co spinels for methane oxidation in presence of s427
Chapter 56. Characterising the porous structure of Egyptian mortars using thermoporometry, mercury i435
Chapter 57. Monitoring fast pressure changes in gas transport and sorption analysis443
Chapter 58. Effect of coke deposition on catalyst texture during catalytic cracking reaction451
Chapter 59. Precision of porosity measurements on cementitious mortars459
Chapter 60. Freezing in mesopores: aniline in silica glasses and MCM-41467
Chapter 61. Transport characteristics of porous solids derived from chromatographic measurements475
Chapter 62. Effects of porous solid structures on the electrical behaviour: prediction key of transp483
Chapter 63. Pore and surface characteristics of porous melamine- and phenolic- formaldehyde polymers491
Chapter 64. Porous structure of multifunctional mineral-carbon and zeolite-carbon sorbents499
Chapter 65. Waste air cleaning using activated carbon fibre cloths regenerable by direct electric he507
Chapter 66. Adsorption of inflammatory cytokines and endotoxin by mesoporous polymers and activated515
Chapter 67. Separation of adsorption isotherms of N2 in internal and interstitial nanopores of singl521
Chapter 68. Visualizing the porous structure of different carbon materials: a scanning tunneling mic529
Chapter 69. Textural characterisation of activated carbons obtained from poly(ethylene terephthalate537
Chapter 70. A Monte Carlo study on the structure of carbon dioxide adsorbed in microporous carbons545
Chapter 71. Preloading of GAC by natural organic matter: effect of surface chemistry on TCE uptake553
Chapter 72. Structural studies of saccharose- and anthracene-based carbons by high-energy X-ray scat561
Chapter 73. The dynamic adsorption behaviour of volatile organic compounds on activated carbon honey569
Chapter 74. Structural properties of Cu-MCM-41 and Cu-Al-MCM-41 (Si/Al=30) catalysts577
Chapter 75. Comparative study of the textural properties of alumina-pillared saponites synthesised f585
Chapter 76. Chord length distribution and pore size distribution of porous VYCOR glass593
Chapter 77. A structural study of dehydration/rehydration of tobermorite, a model cement compound601
Chapter 78. Support mesoporosity: a tool for better control of catalytic behavior of cobalt supporte609
Chapter 79. Textural characterization of montmoriHonite pillared with aluminum/lanthanum polyoxycati617
Chapter 80 .Influence of pH in mesoporous silica aluminas (MSA) synthesis625
Chapter 81. The adsorption of l-hexene and 3,3-dimethyl-l-butene on Ru-MCM 41633
Chapter 82. XPS studies of MCM 41 postmodified by a Schiff base copper complex639
Chapter 83. Influence of synthesis conditions on surface heterogeneity of M41 type materials studied647
Chapter 84. Porosity of chemically modified silica gels by nitrogen adsorption, positron annihilatio655
Chapter 85. Preparation and characterization of porous sorbents for hot gas desulfurization663
Chapter 86. Synthesis and characterization of MWW zeolites671
Chapter 87. Structural analysis of oxyanion-cation complexes anchored by organic group in mesoporous677
Chapter 88. Adsorption equilibrium of polar/non-polar mixtures on MCM-41: experiments and Monte Carl685
Chapter 89. Nondestructive characterization of porous ceramics by X-ray refraction693
Chapter 90. lon-exchange properties of a novel layered titanium(IV) phosphate701
Chapter 91. The anomalous sorptive behaviour of ZSM-5 and Silicalite-l: observation of low pressure709
Chapter 92. Characterization of the textural properties of chemically dealuminated Y zeolites717
Chapter 93. Complementarity of microcalorimetry, manometry and gravimetry in the study of gas adsorp723
Chapter 94. The applicability of the Dubinin-Radushkevich equation to the very low pressure region o731
Chapter 95. Controlled porosity and surface area titania gels as novel photocatalytic washcoats737
Chapter 96. The effect of geometry and axial orientation of spheroidal particles on the adsorption r745
Chapter 97. The effect of Peclet on the Sherwood number in high porosity granular media753
Chapter 98. The application of Jäntti's method for the fast calculation of equilibrium in case of m761
Chapter 99. Characterization of controlled pore glasses by small angle X-ray scattering and evaluati769
Author Index775
Other volumes in the series781

Book details

Vendor Elsevier S & T
SKU 9780444512611
ISBN-13 9780080528915
Author Rodríguez-Reinoso, F.
Category Science
Subject Industrial & Technical

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This book contains 99 of the papers that were presented at the 6th in the series of Symposia on Characterization of Porous Solids held in Alicante, Spain, May 2002.

Written by leading international specialists in the subject, the contributions represent an up-to-date and authoritative account of recent developments around the world in the major methods used to characterize porous solids. The book is a useful work of reference for anyone interested in characterizing porous solids, such as MCM-41 mesoporous materials, pillared clays, etc. Papers on pore structure determination using gas adsorption feature strongly, together with papers on small angle scattering methods, mercury porosimetry, microcalorimetry, scanning probe microscopies, and image analysis.

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