Elsevier S & T

Characterization of Porous Solids VII: Proceedings of the 7th International Symposium on the Characterization of Porous Solids (COPS-VII), Aix-en-Provence, France, 26-28 May 2005

Llewellyn, Philip; Rodríguez Reinoso, Francisco; Rouqerol, Jean; Seaton, Nigel

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Table of contents
  • Cover
  • Forewardv
  • Table of Contentsvii
  • Effect of pore morphology and topology on capillary condensation in nanoporei: a theoretical and mol1
  • 1. ABSTRACT1
  • 2. INTRODUCTION1
  • 3. COMPUTATIONAL DETAILS5
  • 4. RESULTS AND DISCUSSION5
  • 5. CONCLUSION7
  • REFERENCES8
  • Density Functional Theory Model of Adsorption on Amorphous and Microporous Solids9
  • 1. INTRODUCTION9
  • 2. THEORY11
  • 3. RESULTS AND DISCUSSION12
  • 4. CONCLUSIONS15
  • ACKNOWLEDGMENTS15
  • REFERENCES16
  • Thickness of Adsorbed Nitrogen Films in SBA-15 Silica from Small-Angle Neutron Diffraction17
  • 1. INTRODUCTION17
  • 2. EXPERIMENTAL18
  • 3. THEORETICAL BACKGROUND19
  • 3. RESULTS20
  • 4. DISCUSSION22
  • REFERENCES24
  • Strong light scattering upon capillary condensation in silica aerogels25
  • 1. INTRODUCTION25
  • 2. EXPERIMENTAL25
  • 3. RESULTS26
  • 4. DISCUSSION31
  • 5. CONCLUSIONS31
  • REFERENCES32
  • Characterisation of porous solids from nanometer to micrometer range by capillary condensation33
  • 1. INTRODUCTION33
  • 2. EXPERIMENTAL ASPECTS34
  • 3. RESULTS AND DISCUSSION37
  • 4. CONCLUSION39
  • Acknowledgements40
  • REFERENCES40
  • Characterization of zeolite membrane quality by using permporosimetry41
  • 1. INTRODUCTION41
  • 2. EXPERIMENTAL42
  • 3. RESULTS AND DISCUSSION44
  • 4. CONCLUSION48
  • REFERENCE48
  • Is the BET equation applicable to microporous adsorbents?49
  • 1. INTRODUCTION49
  • 2. WHY NOT SIMPLY USE THE LANGMUIR EQUATION WHEN THE ADSORBENT IS KNOWN TO BE MICROPOROUS?49
  • 2. WHY IS THE BET METHOD ALSO LIMITED IN CASE OF MICROPOROUS MATERIALS?50
  • 3. IS THE BET "MONOLAYER CAPACITY" OF A MICROPOROUS MATERIAL A REPRODUCIBLE QUANTITY?50
  • 4. IS THE BET APPROACH REASONABLY SUPPORTED BY CALORIMETRY?52
  • 5. FINALLY, IN THE PRESENCE OF MICROPORES, CAN THE BET EQUATION BE MEANINGFUL AND USEFUL?54
  • 6. CONCLUSIONS55
  • REFERENCES56
  • A new classification of pore sizes57
  • 1. INTRODUCTION57
  • 2. BACKGROUND57
  • 3. NEW PORE SIZE CLASSSIFICATION59
  • 4. CONCLUDING REMARKS61
  • ACKNOWLEDGEMENTS61
  • REFERENCES62
  • Characterization of nanoporous carbons63
  • 1. INTRODUCTION63
  • 2. THEORY64
  • 3. EXPERIMENTAL65
  • 4. RESULTS AND DISCUSSION66
  • 5. CONCLUSIONS70
  • 6. ACKNOWLEDGEMENT70
  • REFERENCES70
  • Adsorption and neutron scattering studies: a reliable way to characterize both the mesoporous MCM-4171
  • 1. INTRODUCTION71
  • 2. EXPERIMENTAL SECTION72
  • 3. RESULTS AND DISCUSSION72
  • 4. CONCLUSION78
  • REFERENCES78
  • Absolute assessment of adsorption-based microporous solid characterisation methods79
  • 1. INTRODUCTION79
  • 2. ABSOLUTE ASSESSMENT METHODOLOGY79
  • 3. STUDY DETAILS80
  • 4. RESULTS AND DISCUSSION82
  • 5. CONCLUSIONS85
  • ACKNOWLEDGEMENTS86
  • REFERENCES86
  • Molecular Modeling of Mercury Porosimetry87
  • Abstract87
  • 1. Introduction87
  • 2. Models and Methods88
  • 3. Application to porous glasses90
  • 4. Conclusions93
  • Acknowledgement94
  • REFERENCES94
  • Predicting ambient temperature adsorption of gases in active carbons95
  • ABSTRACT95
  • 1. INTRODUCTION95
  • 2. MOLECULAR MODELS96
  • 3. PREDICTION OF PURE GAS ADSORPTION98
  • 4. DISCUSSION102
  • REFERENCES103
  • Characterisation of periodic mesoporous silicas using molecular simulation105
  • 1 INTRODUCTION105
  • 2 KINETIC MONTE CARLO-BASED MODEL FOR MCM-41106
  • 3 PORE NETWORK MODEL FOR SBA-2108
  • 4 DISCUSSION111
  • ACKNOWLEDGEMENTS111
  • REFERENCES111
  • Structural characterization of porous carbonaceous materials using high-pressure adsorption measurem113
  • 1. INTRODUCTION113
  • 2. THEORITICAL DEVELOPMENT114
  • 3. RESULTS AND DISCUSSION118
  • 4. SUMMARY AND CONCLUSIONS120
  • REFERENCES120
  • Microcalorimetric Characterization of Hydrogen Adsorption on Nanoporous Carbon Materials121
  • 1. INTRODUCTION121
  • 2. EXPERIMENTAL122
  • 3. RESULTS AND DISCUSSION122
  • 4. CONCLUSION128
  • ACKNOWLEDGEMENTS128
  • REFERENCES128
  • Effect of thermal treatments on the surface chemistry of oxidized activated carbons129
  • 1. INTRODUCTION129
  • 2. EXPERIMENTAL130
  • 3. RESULTS AND DISCUSSION130
  • 4. CONCLUSIONS135
  • REFERENCES136
  • Digital reconstruction of silica gels based on small angle neutron scattering data137
  • 1. ABSTRACT137
  • 2. INTRODUCTION137
  • 3. MATERIALS138
  • 4. SMALL ANGLE NEUTRON SCATTERING138
  • 5. DIGITAL REPRESENTATION OF THE STRUCTURE OF BIPHASIC MEDIA140
  • 6. DETERMINATION OF SORPTION PROPERTIES (S4 gel)142
  • 7. CONCLUSIONS143
  • REFERENCES144
  • The impact of mesoporosity on microporosity assessment by CO2 adsorption, revisited145
  • 1. INTRODUCTION145
  • 2. EXPERIMENTAL147
  • 3. RESULTS AND DISCUSSION148
  • 4. CONCLUSIONS152
  • Acknowledgements152
  • REFERENCES152
  • A Monte Carlo study of capillary condensation of krypton within realistic models of templated mesopo153
  • 1. ABSTRACT153
  • 2. INTRODUCTION153
  • 2. SIMULATION DETAILS154
  • 3. RESULTS155
  • 4. CONCLUSIONS159
  • REFERENCES160
  • Using molecular simulation to characterise metal-organic frameworks and judge their performance as a161
  • 1. INTRODUCTION161
  • 2. SIMULATION DETAILS162
  • 3. RESULTS163
  • 4. CONCLUSIONS167
  • ACKNOWLEDGEMENTS168
  • REFERENCES168
  • Stability of Porous Carbon Structures Obtained from Reverse Monte Carlo using Tight Binding and Bond169
  • 1. INTRODUCTION169
  • 2. COMPUTATIONAL METHODOLOGY170
  • 3. RESULTS AND DISCUSSION171
  • 4. CONCLUSIONS175
  • 5. ACKNOWLEDGEMENTS176
  • 6. REFERENCES176
  • Simulation of mercury porosimetry using MRI images of porous media177
  • Abstract177
  • 1. INTRODUCTION177
  • 2. THEORY178
  • 3. EXPERIMENTAL180
  • 4. RESULTS AND DISCUSSION181
  • 5. CONCLUSIONS184
  • REFERENCES184
  • Adsorption and microcalorimetric measurements on activated carbons prepared from Polyethylene Tereph185
  • 1. ABSTRACT185
  • 2. INTRODUCTION185
  • 3. EXPERIMENTAL186
  • 4. RESULTS AND DISCUSSION187
  • CONCLUSIONS192
  • ACKNOWLEDGEMENTS192
  • REFERENCES192
  • Compressing some sol-gel materials reduces their stiffness: a textural analysis193
  • 1. INTRODUCTION193
  • 2. EXPERIMENTAL SECTION194
  • 3. RESULTS195
  • 4. DISCUSSION197
  • 5. CONCLUSIONS200
  • Acknowledgements200
  • REFERENCES200
  • Characterisation of new Pd / hierarchical maero-mesoporous ZrO2, TiO2 and ZrO2-TiO2 catalysts for to201
  • 1. INTRODUCTION201
  • 2. SYNTHESIS AND CHARACTERISATIONS202
  • CONCLUSION208
  • ACKNOWLEDGEMENTS208
  • REFERENCES208
  • Characterisation of palladium supported on exchanged BEA and FAII zeolites for VOCs catalytic oxidat209
  • 1. INTRODUCTION209
  • 2. EXPERIMENTAL209
  • 3. RESULTS AND DISCUSSIONS211
  • 4. CONCLUSION216
  • ACKNOWLEDGEMENTS216
  • REFERENCES216
  • Comparison of transport characteristics and textural properties of porous material; the role of pore217
  • ABSTRACT217
  • 1. INTRODUCTION217
  • 2. EXPERIMENTAL218
  • 3. RESULTS AND DISCUSSION221
  • 4. CONCLUSIONS223
  • ACKNOWLEDGEMENT223
  • Effect of noble metal deposition in zeolitic structures on their adsorption capacities225
  • 1. INTRODUCTION225
  • 2. MATERIALS SYNTHESIS AND CHARACTERISATION226
  • 3. ADSORPTION STUDY227
  • 4. CONCLUSIONS232
  • 5. ACKNOWLEDGMENTS232
  • REFERENCES232
  • Influence of the Bentonite/Titania ratio on the textural characteristics of incorporated ceramics fo233
  • 1. INTRODUCTION233
  • 2. EXPERIMENTAL234
  • 3. RESULTS AND DISCUSSION235
  • 4. CONCLUSIONS239
  • Acknowledgements239
  • REFERENCES239
  • Simultaneous Determination of Intrinsic Adsorption and Diffusion of n-Butane in Activated Carbons by241
  • 1. INTRODUCTION241
  • 2. MATERIAL AND METHODS242
  • 3. RESULTS244
  • 4. DISCUSSION245
  • 5. CONCLUSIONS247
  • ACKNOWLEDGEMENTS247
  • REFERENCES247
  • Porous carbon deposits in controlled fusion reactor: adsorption properties and structural characteri249
  • 1. INTRODUCTION249
  • 2. EXPERIMENTAL PART AND METHODS249
  • 3. RESULTS AND DISCUSSION:251
  • 4. CONCLUSION255
  • REFERENCES256
  • Characterization of the porosity of a microporous model carbon257
  • 1. INTRODUCTION257
  • 2. THE MODEL CARBON258
  • 3. THE REAL PSD OF THE MODEL CARBON BY ETHING PROCEDURE258
  • 4. ANALYSIS OF THE MODEL CARBON IN TERMS OF THE INTERSECTING CAPPILLARIES MODEL258
  • 5. RESULTS AND DISCUSSION260
  • 5. CONCLUSIONS264
  • ACKNOWLEDGEMENT264
  • REFERENCES264
  • Qualitative assessment of the purity of multi-walled carbon nanotube samples using krypton adsorptio265
  • 1. INTRODUCTION265
  • 2. EXPERIMENTAL SECTION266
  • 3. RESULTS AND DISCUSSION268
  • 4. CONCLUSION270
  • Acknowledgements271
  • REFERENCES271
  • Study of the Anomalous Behaviour of MFI Zeolites Towards Nitrogen Adsorption273
  • 2. INTRODUCTION273
  • 3. EXPERIMENTAL274
  • 4. RESULTS AND DISCUSSION274
  • REFERENCES278
  • Characterization of alkaline post-treated ZSM-5 zeolites by low temperature nitrogen adsorption279
  • 1. INTRODUCTION279
  • 2. EXPERIMENTAL280
  • 3. RESULTS AND DISCUSSION281
  • 4. CONCLUSIONS284
  • ACKNOWLEDGMENTS284
  • REFERENCES285
  • Kureha activated carbon characterized by the adsorption of light hydrocarbons287
  • 1. INTRODUCTION287
  • 2. EXPERIMENTAL288
  • 3. RESULTS AND DISSCUSSION289
  • 4. CONCLUSIONS294
  • REFERENCES294
  • Water adsorption/desorption isotherms for characterization of microporosity in sandstone and carbona295
  • 1. INTRODUCTION295
  • 2. EXPERIMENTAL296
  • 3. RESULTS AND DISCUSSION298
  • 4. CONCLUSION301
  • ACKNOWLEDGEMENTS302
  • REFERENCES302
  • Determination of pore-size distributions of highly-connected networks with assisted-filling characte303
  • 1. INTRODUCTION303
  • 2. SIMULATION OF 3-D POROUS NETWORKS306
  • 3. N2 SORPTION RESULTS307
  • 4. MERCURY POROSIMETRY RESULTS308
  • 5. CONCLUSIONS310
  • REFERENCES310
  • Large-scale simulations of poly(propylene oxide)amine/Na+-montmorillonite and poly(propylene oxide).311
  • 1. INTRODUCTION311
  • 2. METHODOLOGY312
  • 3. RESULTS313
  • 4. DISCUSSION316
  • 5. CONCLUSION317
  • ACKNOWLEDGEMENTS317
  • REFERENCES317
  • A comparison of characterization methods based on N2 and CO2 adsorption for the assessment of the po319
  • 1. INTRODUCTION319
  • 2. EXPERIMENTAL320
  • 3. RESULTS AMD DISCUSSION321
  • 4. CONCLUSIONS325
  • REFERENCES326
  • Adsorption of nitrogen, hydrogen and carbon dioxide on alumina-pillared clays327
  • 1. INTRODUCTION327
  • 2. EXPERIMENTAL328
  • 3. RESULTS AND DISCUSSION329
  • 4. SUMMARY AND CONCLUSIONS332
  • 5. ACKNOWLEDGEMENTS332
  • REFERENCES334
  • CH4 adsorption in Faujasite systems: Microcalorimetry and Grand Canonical Monte Carlo simulations335
  • 1. INTRODUCTION335
  • 2. EXPERIMENTAL336
  • 3. COMPUTATIONAL METHODOLOGY337
  • 4. RESULTS AND DISCUSSIONS338
  • CONCLUSIONS341
  • REFERENCES342
  • Amino-functionalized low density silica xerogels seen by different characterization methods343
  • 1. INTRODUCTION343
  • 2. EXPERIMENTAL343
  • 3. RESULTS AND DISCUSSION345
  • 4. CONCLUSIONS349
  • ACKNOWLEDGMENT350
  • REFERENCES350
  • CO2 adsorption in synthetic hard carbons351
  • 1. INTRODUCTION351
  • 2. EXPERIMENTAL351
  • 3. RESULTS352
  • 4. DISCUSSION355
  • 5. SUMMARY AND CONCLUSIONS355
  • REFERENCES356
  • Characterisation of Nanoporous Aluminosilicate Monoliths Derivatised with Metal Cations for Selectiv357
  • 1. INTRODUCTION357
  • 2. EXPERIMENTAL358
  • 3. RESULTS AND DISCUSSIONS359
  • Acknowledgments364
  • REFERENCES364
  • Comparison of nitrogen and carbon dioxide as molecular probes of low surface area carbonaceous mater365
  • 1. INTRODUCTION365
  • 2. METHODOLOGY366
  • 3. RESULTS369
  • 4. DISCUSSION373
  • ACKNOWLEDGEMENT374
  • REFERENCES374
  • Water sorption in hydrophobic porous materials: isotherm shapes and their meanings for the mesoporou375
  • 1. INTRODUCTION375
  • 2. EXPERIMENTAL SECTION377
  • 3. RESULTS377
  • 4. CONCLUSIONS381
  • REFERENCES382
  • Uncertainty in alpha s analyses and pore volumes propagated from uncertainty in gas adsorption data383
  • 1. INTRODUCTION383
  • 2. EXPERIMENTAL384
  • 3. UNCERTAINTY IN alphaS-DATA AND PORE VOLUMES384
  • 4. CONCLUSION388
  • ACKNOWLEDGEMENT388
  • REFERENCES388
  • Uncertainty in amount adsorbed and surface excess from uncertainty in high-pressure gas adsorption d389
  • 1. INTRODUCTION389
  • 2. EXPERIMENTAL390
  • 3. RESULTS AND DISCUSSIONS391
  • 4. CONCLUSIONS395
  • ACKNOWLEDGEMENT395
  • REFERENCES396
  • A new methodology to characterize the porosity of Y zeolites by liquid chromatography397
  • 1. INTRODUCTION397
  • 2. METHODOLOGY397
  • 3. EXPERIMENTAL400
  • 4. RESULTS AND DISCUSSION403
  • 5. CONCLUSIONS406
  • REFERENCES406
  • Study of the microporous texture of active carbons by Small Angle Neutron Scattering407
  • INTRODUCTION407
  • 1. PREPARATION AND ADSORPTIOMETRY407
  • 2. EXPERIMENTS408
  • 3. DISCUSSION409
  • CONCLUSION413
  • REFERENCES413
  • Characterisation of nanostructured materials by combination of neutron scattering and 3D stochastic415
  • 1. INTRODUCTION415
  • 2. EXPERIMENTAL416
  • 3. EVALUATION OF THE SCATTERING DATA417
  • 4. REPRESENTATION OF THE POROUS STRUCTURE417
  • 5. RELATION BETWEEN SANS SPECTRUM AND AUTOCORRELATION FUNCTION418
  • 6. STOCHASTIC RECONSTRUCTION418
  • 7. CALCULATION OF PERMEABILITY420
  • CONCLUSIONS421
  • Acknowledgements421
  • REFERENCES422
  • Hydrogen storage in nanoporous carbons423
  • 1. INTRODUCTION423
  • 2. EXPERIMENTAL DETAILS424
  • 3. MONTE CARLO SIMULATION425
  • 4. RESULTS AND DISCUSSION426
  • 5. CONCLUDING REMARKS430
  • ACKNOWLEDGEMENTS430
  • REFERENCES430
  • Migration of siloxane polymer in ordered mesoporous MCM-41 silica channels431
  • 1. INTRODUCTION431
  • 2. EXPERIMENTAL432
  • 3. RESULTS AND DISCUSSION433
  • 4. CONCLUSIONS437
  • REFERENCES437
  • The sorption dynamics of propane, i-butane and neopentane in carbon nanotubes439
  • 1. INTRODUCTION439
  • 2. EXPERIMENTAL SECTION440
  • 3. RESULTS AND DISCUSSION441
  • 4. CONCLUSION445
  • ACKNOWLEDGEMENTS446
  • REFERENCES446
  • Adsorption and diffusion kinetics of alkanes (C3 & C5) on different CaA adsorbents447
  • 1. INTRODUCTION447
  • 2. EXPERIMENTAL447
  • 3. RESULTS AND DISCUSSION448
  • CONCLUSION452
  • REFERENCES453
  • Transport properties of catalyst supports derived from a catalytic test reaction455
  • 1. INTRODUCTION455
  • 2. EXPERIMENTAL456
  • 3. RESULTS AND DIS457
  • 4. CONCLUSIONS462
  • REFERENCES462
  • Ellipsometric study of porosity distribution in hybrid silica-based sol-gel films463
  • 1. INTRODUCTION463
  • 2. EXPERIMENTAL463
  • 3. RESULTS AND DISCUSSION464
  • 4. CONCLUSIONS469
  • REFERENCES469
  • Positronium annihilation study of as-synthesized MCM-41 silica under pressure471
  • 1. INTRODUCTION471
  • 2. EXPERIMENTAL472
  • 3. RESULTS AND DISCUSSION472
  • 4. CONCLUSIONS478
  • REFERENCES478
  • Structure-adsorptive characteristics of template-based mesoporous silicas containing residues of som479
  • 1. INTRODUCTION479
  • 2. MATERIALS AND METHODS479
  • 3. RESULTS AND DISCUSSION481
  • 4. CONCLUSIONS485
  • ACKNOWLEDGMENT485
  • REFERENCES485
  • Melting of atomic layers in carbon nanotubes487
  • 1. INTRODUCTION487
  • 2. MELTING ALONG ISOTHERMS488
  • 3. THERMODYNAMIC PATHS OF MELTING489
  • 4. INFLUENCE OF THE WALL CORRUGATION ON THE MECHANISM OFMELTING491
  • 5. CONCLUSIONS492
  • REFERENCES494
  • Molecular simulation study on the structure of templated porous materials obtained from different in495
  • 1. INTRODUCTION495
  • 2. MODEL496
  • 3. SIMULATION METHOD497
  • 4. RESULTS AND DISCUSSION497
  • 5. CONCLUSIONS501
  • ACKNOWLEDGMENTS502
  • REFERENCES502
  • The structure of high-pressure adsorbed fluids in slit-pores503
  • 1. INTRODUCTION503
  • 2. THEORY504
  • 3. SIMULATION505
  • 4. RESULTS AND DISCUSSION505
  • 5. CONCLUSIONS508
  • REFERENCES509
  • Monte Carlo simulation of the isosteric heats - implications for the characterisation of porous mate511
  • 1. INTRODUCTION512
  • 2. ABSOLUTE AND EXCESS ADSORPTION512
  • 3. THE ISOSTERIC HEAT AND THE PSD514
  • 4. MOLECULAR MODELS515
  • 5. RESULTS AND DISCUSSION515
  • 6. CONCLUSIONS518
  • ACKNOWLEDGEMENT518
  • REFERENCES518
  • Pore size distribution in microporous carbons obtained from molecular modeling and density functiona519
  • 1. INTRODUCTION519
  • 2. THEORETHICAL APPROACH520
  • 3. EXPERIMENTAL METHOD521
  • 4. RESULTS522
  • 5. CONCLUSIONS526
  • ACKNOWLEDGMENTS526
  • REFERENCES526
  • Modeling Triblock Surfactant Templated Mesoporous Silicas (MCF and SBA-15): A Mimetic Simulation Stu527
  • 2. INTRODUCTION527
  • 3. SIMULATION DETAILS528
  • 4. RESULTS AND DISCUSSION529
  • 5. CONCLUSIONS534
  • REFERENCES534
  • Influence of temperature on water adsorption / desorption hysteresis loop in disordered mesoporous s535
  • 1. INTRODUCTION535
  • 2. COMPUTATIONAL DETAILS536
  • 3. RESULTS AND DISCUSSIONS539
  • 4. CONCLUSION540
  • ACKNOWLEDGMENT.540
  • REFERENCES540
  • Determination of pore size distribution in microporous carbons based on CO2 and H2 sorption data543
  • 1. INTRODUCTION543
  • 2. EXPERIMENTAL545
  • 3. SIMULATION MODEL545
  • 4. MICROPORE SIZE DISTRIBUTIONS547
  • 5. CONCLUSIONS549
  • REFERENCES550
  • Assessment of the development of the pore size distribution during carbon activation: a population b551
  • 1. INTRODUCTION551
  • 2. PRODUCTION552
  • 3. CHARACTERISATION552
  • 4. POPULATION BALANCE METHOD553
  • 5. RESULTS AND DISCUSSION554
  • 6. CONCLUSIONS558
  • ACKNOWLEDGMENTS558
  • REFERENCES558
  • Chemically modified nanoporous carbons obtained using template carbonization method559
  • 1. INTRODUCTION559
  • 2. EXPERIMENTAL560
  • 3. RESULTS AND DISCUSSION561
  • 4. CONCLUSIONS565
  • Acknowledgments566
  • REFERENCES566
  • Influence of the synthesis conditions on the pore structure and stability of MCM-41 materials contai567
  • 1. INTRODUCTION567
  • 2. EXPERIMENTAL568
  • 3. RESULTS AND DISCUSSION568
  • 4. CONCLUSIONS574
  • Acknowledgements574
  • REFERENCES574
  • Effect of oxidizing agent on activated carbon cloth porosity and surface chemistry575
  • 1. INTRODUCTION575
  • 2. EXPERIMENTAL575
  • 3. RESULTS AND DISCUSSION576
  • 4. CONCLUSIONS582
  • ACKNOWLEDGEMENT582
  • REFERENCES582
  • Study of the efficiency of monolithic activated carbon adsorption units583
  • 1. INTRODUCTION583
  • 2. EXPERIMENTAL584
  • 3. RESULTS AND DISCUSSION586
  • 4. CONCLUSIONS590
  • Acknowledgements590
  • REFERENCES590
  • Amino functionalisation of microemulsion templated mesoporous silica foams591
  • 1. INTRODUCTION591
  • 2. MATERIALS AND METHODS592
  • 3. RESULTS AND DISCUSSION594
  • 4. CONCLUSIONS597
  • ACKNOWLEDGEMENT598
  • REFERENCES598
  • Effect of activation process on resin based activated carbons599
  • 1. INTRODUCTION599
  • 2. EXPERIMENTAL600
  • 3. RESULTS AND DISCUSSION601
  • 4. CONCLUSIONS606
  • References606
  • Highly microporous carbons prepared by activation of kraft lignin with KOH607
  • 1. INTRODUCTION607
  • 2. EXPERIMENTAL608
  • 3. RESULTS AND DISCUSION609
  • 4. CONCLUSIONS613
  • REFERENCES613
  • Preparation and Characterization of Nanoporous Ternary Mixed Cerium Oxides615
  • 1. INTRODUCTION615
  • 2. EXPERIMENTAL616
  • 3. RESULTS AND DISCUSSION617
  • REFERENCES620
  • Preparation and dynamic adsorption properties of activated carbons with tailored micro- and mesoporo621
  • 1. INTRODUCTION621
  • 2. EXPERIMENTAL621
  • 3. RESULTS623
  • 4. DISCUSSION626
  • 5. CONCLUSIONS627
  • REFERENCES628
  • Preparation of functionally graded alumina ceramic materials with controlled porosity629
  • 1. INTRODUCTION629
  • 2. MATERIALS AND METHODS630
  • 3. EXPERIMENT630
  • 4. DISCUSSIONS AND CONCLUSION636
  • ACKNOWLEDGEMENT637
  • REFERENCES637
  • Preparation of Mesoporous Ceria in the Presence of Non-Aqueous Phases639
  • 1. INTRODUCTION639
  • 2. EXPERIMENTAL639
  • 3. RESULTS AND DISCUSSION640
  • REFERENCES644
  • Preparation and Characterization of Nanoporous Solids with Composition CexMn1-xO2-y With x Values 0645
  • 1. INTRODUCTION645
  • 2. EXPERIMENTAL646
  • 3. RESULTS AND DISCUSSION647
  • REFERENCES650
  • Thermal stability of ion exchange and adsorption properties of titania gels prepared from titanous c651
  • 1. INTRODUCTION651
  • 2. EXPERIMENTAL652
  • 3. RESULTS AND DISCUSSION653
  • 4. CONCLUSIONS659
  • ACKNOWLEDGEMENT659
  • RRFERENCES659
  • In-situ SAXS on Transformations of Mesoporous and Nanostructured Solids661
  • 1. INTRODUCTION661
  • 2. THEORY661
  • 3. EXPERIMENTAL663
  • 4. RESULTS AND DISCUSSION663
  • 5. CONCLUSION665
  • REFERENCES665
  • Confinement effects on freezing of binary mixtures667
  • 1. INTRODUCTION667
  • 2. EXPERIMENTAL AND SIMULATION METHODS668
  • 3. RESULTS AND DISCUSSION669
  • 4. CONCLUSIONS674
  • REFERENCES674
  • New equipment for characterization of nanofiltration membranes675
  • 1. INTRODUCTION675
  • 2. MEASURING PROCEDURE AND EXAMPLES OF RESULTS676
  • 3. CONCLUSION679
  • REFERENCES680
  • The porous structure of biodegradable scaffolds obtained with supercritical CO2 as foaming agent681
  • ABSTRACT681
  • 1. INTRODUCTION681
  • 2. MATERIAL AND METHODS682
  • 3. RESULTS683
  • 4. DISCUSSION686
  • ACKNOWLEDGEMENTS687
  • REFERENCES687
  • Detection of specific electronic interactions at the interface aromatic hydrocarbon-graphite by imme689
  • 1. INTRODUCTION689
  • 2. EXPERIMENTAL690
  • 3. RESULTS AND DISCUSSION691
  • ACKNOWLEDGEMENT695
  • REFERENCES695
  • Characterization and modelling of argillaceous porous medium by compressional and shear acoustic wav697
  • 1. INTRODUCTION697
  • 2. THEORITECAL BACKGROUND697
  • 3. RESULTS AND DISCUSSION699
  • EXAMPLE OF P AND S VELOCITIES MODELLING IN ARGILLACEOUS SEDIMENTS702
  • 5. CONCLUSION703
  • REFERENCES704
  • Modelisation and circulation of fluids in geological porous systems. Images analyzing and mercury po705
  • 1. INTRODUCTION705
  • 2. MATERIALS AND METHODS706
  • 3. THEORY706
  • 4. FLUID PROGRESSION SIMULATION IN POROUS SURFACE IMAGE707
  • 5. RESULTS710
  • 6. CONCLUSION AND PROSPECTS712
  • REFERENCES712
  • Electrical behaviour of saturated and unsaturated geological carbonate porous systems713
  • I. INTRODUCTION713
  • II. THEORETICAL BACKGROUND714
  • III. SAMPLE DATA BASE715
  • IV. EXPERIMENTAL SETTING AND PROCEDURES715
  • V. RESULTS AND DISCUSSIONS717
  • VI. CONCLUSION719
  • REFERENCES719
  • Author Index721
  • Studies in Surface Science and Catalysis725
Book details
  • Vendor Elsevier S & T
  • SKU 9780444520227
  • ISBN-13 9780080463711
  • Author Llewellyn, Philip; Rodríguez Reinoso, Francisco; Rouqerol, Jean; Seaton, Nigel
  • Category Technology & Engineering
  • Subject Materials Science

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The 7th International Symposium on the Characterization of Porous Solids (COPS-VII) was held in the Congress Centre in Aix-en-Provence between the 25th-28th May 2005.
The symposium covered recent results of fundamental and applied research on the characterization of porous solids. Papers relating to characterization methods such as gas adsorption and liquid porosimetry, X-ray techniques and microscopic measurements as well as the corresponding molecular modelling methods were given. These characterization methods were shown to be applied to all types of porous solids such as clays, carbons, ordered mesoporous materials, porous glasses, oxides, zeolites and metal organic frameworks.

* 36 oral presentations and 166 posters and around 230 guests from 27 countries.
* A large part of this symposium was devoted to the use computational methods to characterise porous solids