Elsevier S & T

Handbook of Thermal Analysis and Calorimetry: Principles and Practice

Brown, Michael E.

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Table of contents
  • CONTENTSix
  • Forewordv
  • Prefacevii
  • Contributorsxxix
  • CHAPTER 1. DEFINITIONS, NOMENCLATURE, TERMS AND LITERATURE1
  • 1. INTRODUCTION1
  • 2. THERMAL ANALYSIS AND CALORIMETRY- DEFINITIONS, CLASSIFICATIONS AND NOMENCLATURE7
  • 3. CHARACTERIZATION OF MEASURING INSTRUMENTS31
  • 4. CHARACTERIZATION OF MEASURED CURVES AND VALUES36
  • 5. CHARACTERIZATION, INTERPRETATION AND PRESENTATION OF RESULTS41
  • 6. LITERATURE ON THERMAL ANALYSIS AND CALORIMETRY49
  • Acknowledgement72
  • References72
  • CHAPTER 2. THERMODYNAMIC BACKGROUND TO THERMAL ANALYSIS AND CALORIMETRY75
  • 1. INTRODUCTION75
  • 2. THERMODYNAMIC SYSTEMS AND THE CONCEPT OF TEMPERATURE76
  • 3. THE FIRST LAW OF THERMODYNAMICS82
  • 4. THE SECOND AND THE THIRD LAWS OF THERMODYNAMICS91
  • 5. THE HELMHOLTZ ENERGY AND THE GIBBS ENERGY95
  • 6. EQUILIBRIUM CONDITIONS98
  • 7. OPEN SYSTEMS103
  • 8. SYSTEMS CONSISTING OF A PURE SUBSTANCE106
  • 9. MIXTURES AND PHASE DIAGRAMS119
  • 10. CHEMICAL REACTIONS136
  • References144
  • CHAPTER 3 . KINETIC BACKGROUND TO THERMAL ANALYSIS AND CALORIMETRY147
  • 1. INTRODUCTION147
  • 2. KINETIC MODELS FOR SOLID-STATE REACTIONS150
  • 3. THE MOST IMPORTANT RATE EQUATIONS USED IN KINETIC ANALYSES OF SOLID STATE REACTIONS172
  • 4. KINETIC ANALYSIS OF ISOTHERMAL EXPERIMENTS172
  • 5. THE INFLUENCE OF TEMPERATURE ON REACTION RATE179
  • 6. KINETIC ANALYSIS OF NON-ISOTHERMAL EXPERIMENTS185
  • 7. KINETIC ASPECTS OF NON-SCANNING CALORIMETRY209
  • 8. PUBLICATION OF KINETIC RESULTS214
  • References216
  • CHAPTER 4. THERMOGRAVIMETRY AND THERMOMAGNETOMETRY225
  • 1. INTRODUCTION225
  • 2. MEASUREMENT OF MASS227
  • 3. DESIGN AND CONTROL OF THE THERMOBALANCE237
  • 4. DATA COLLECTION AND PRESENTATION263
  • 5. CALIBRATION268
  • References275
  • CHAPTER 5. DIFFERENTIAL THERMAL ANALYSIS AND DIFFERENTIAL SCANNING CALORIMETRY279
  • 1. INTRODUCTION AND HISTORICAL BACKGROUND279
  • 2. DEFINITIONS AND DISTINCTIONS284
  • 3. THEORY OF DTA AND DSC288
  • 4. INSTRUMENTATION299
  • 5. MODULATED TEMPERATURE DIFFERENTIAL SCANNING CALORIMETRY (MTDSC)321
  • 6. OPERATIONS AND SAMPLING334
  • 7. GENERAL INTERPRETATION AND CONCLUSIONS345
  • References355
  • CHAPTER 6. THERMOMECHANICAL METHODS363
  • 1. INTRODUCTION363
  • 2. STATIC METHODS363
  • 3. DYNAMIC MECHANICAL THERMAL ANALYSIS (DMTA)373
  • 4. CONCLUSION398
  • References398
  • CHAPTER 7. DIELECTRIC TECHNIQUES401
  • 1. INTRODUCTION401
  • 2. DILECTRIC RESPONSE401
  • 3. TEMPERATURE DEPENDENCE413
  • 4. EFFECT OF MOISTURE CONTENT416
  • 5. INSTRUMENTATION416
  • NOMENCLATURE421
  • References422
  • CHAPTER 8. CONTROLLED RATE THERMAL ANALYSIS AND RELATED TECHNIQUES423
  • 1. INTRODUCTION423
  • 2. HISTORICAL DEVELOPMENT423
  • 3. DIFFERENT PROPERTIES AND MODES USED FOR SCTA428
  • 4. NOMENCLATURE429
  • 5. THE ADVANTAGES OF SCTA430
  • 6. KINETIC ASPECTS434
  • 7. PROSPECTS FOR THE FUTURE439
  • 8. CONCLUSIONS440
  • References441
  • CHAPTER 9. LESS-COMMON TECHNIQUES445
  • 1. INTRODUCTION445
  • 2. EMANATION THERMAL ANALYSIS (ETA)445
  • 3. THERMOSONIMETRY460
  • 4. THERMOACOUSTIMETRY465
  • 5. MISCELLANEOUS469
  • References469
  • CHAPTER 10. THERMOMICROSCOPY473
  • 1. HISTORICAL INTRODUCTION473
  • 2. GENERAL EQUIPMENT AND ACCESSORIES474
  • 3. EXPERIMENTAL METHODS478
  • 4. EXAMPLES OF APPLICATIONS481
  • 5. CONCLUSIONS494
  • 6. ACKNOWLEDGEMENTS494
  • References494
  • CHAPTER 11. SIMULTANEOUS MEASUREMENTS497
  • 1. INTRODUCTION497
  • 2. SIMULTANEOUS THERMO GRAVIMETRY-DIFFERENTIAL SCANNING CALORIMETRY TG-DSC (DTA)498
  • 3. SIMULTANEOUS THERMOMECHANICAL ANALYSIS- DIFFERENTIAL THERMAL ANALYSIS (TMA-DTA)503
  • 4. SIMULTANEOUS DIFFERENTIAL SCANNING CALORIMETRY- THERMOPTOMETRY (DSC-TOA)505
  • 5. SIMULTANEOUS DYNAMIC MECHANICAL ANALYSIS- DIELECTRIC THERMAL ANALYSIS (DMA-DETA)506
  • 6. OTHER TECHNIQUES507
  • ACKNOWLEDGEMENTS507
  • References507
  • CHAPTER 12. EGA- EVOLVED GAS ANALYSIS509
  • 1. INTRODUCTION509
  • 2. COUPLING TG-MS509
  • 3. COUPLING TG-FTIR518
  • 4. THE USE OF ANALYTICAL TECHNIQUES BY ON-LINE AND OFF-LINE COMBINATION WITH THERMAL ANALYSIS526
  • References541
  • CHAPTER 13. CALIBRATION AND STANDARDISATION IN DSC547
  • 1. INTRODUCTION547
  • 2. TEMPERATURE CALIBRATION548
  • 3. CALORIMETRIC CALIBRATION556
  • 4. REFERENCE MATERIALS561
  • 5. CONCLUDING REMARKS573
  • References573
  • CHAPTER 14. NONSCANNING CALORIMETRY577
  • 1. INTRODUCTION577
  • 2. DEFINITIONS AND EXPLANATIONS579
  • 3. SYSTEMATIC ERRORS586
  • 4. TEST AND CALIBRATION PROCEDURES591
  • 5. CALORIMETRY SCIENCES CORPORATION AND RELATED CALORIMETERS595
  • 6. SCERES CALORIMETERS609
  • 7. SETARAM CALORIMETERS618
  • 8. THERMOMETRIC CALORIMETERS634
  • 9. SOME OTHER COMMERCIALIZED DESIGNS652
  • 10. COMBUSTION CALORIMETERS657
  • ACKNOWLEDGMENTS669
  • References670
  • INDEX677
Book details
  • Vendor Elsevier S & T
  • SKU 9780444820853
  • ISBN-13 9780080539591
  • Author Brown, Michael E.
  • Category Science
  • Subject Analytic

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Handbook of Thermal Analysis and Calorimetry