Inductively Coupled Plasma-Mass Spectrometry: Practices and Techniques
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Table of contents
- Cover
- Coppyright Pageiv
- Contentsvii
- About the Authorxi
- Chapter 1. Introduction1
- 1.1 History2
- 1.2 Overview3
- Chapter 2. Atomic Structure7
- 2.1 Bohr Model8
- 2.2 Isotopes10
- Chapter 3. Inductively Coupled Plasmas15
- 3.1 Plasma Formation16
- 3.2 Plasma Configuration23
- Chapter 4. Instrumentation29
- 4.1 Interface30
- 4.2 Ion Lenses31
- 4.3 Mass Spectrometers34
- 4.4 Detectors47
- Chapter 5. Sample Introduction53
- 5.1 Gaseous Samples55
- 5.2 Liquid Samples62
- 5.3 Solid Samples79
- Chapter 6. Special Techniques91
- 6.1 Flow Injection91
- 6.2 Chromatography95
- 6.3 Field Flow Fractionation98
- Chapter 7. Quantitation Techniques103
- 7.1 Qualitative Analysis104
- 7.2 Semiquantitative Analysis106
- 7.3 Quantitative Analysis108
- Chapter 8. Interfrences125
- 8.1 Spectrometric Effects126
- 8.2 Nonspectrometric Effects137
- Chapter 9. Optimization143
- 9.1 Parameter Optimization144
- 9.2 Cold PlasmaŽ Operating Conditions147
- Chapter 10. Figures of Merit149
- 10.1 Sensitivity150
- 10.2 Detection Limits151
- 10.3 Precision155
- 10.4 Accuracy157
- References161
- Appendix 1. Table of Elements with Atomic Number, Weights, and First and Second Ionization Potential163
- Appendix 2. Isotopic Composition of the Elements167
- Appendix 3. Prominent Polyatomic In terferences Applicable for ICP-MS Determinations175
- Appendix 4. Table of Student’s t Distribution179
- Appendix 5. Certified Standard Reference Materials Available from the U.S. NIST and the NRC of Canad181
- Appendix 6. Supplemental References187
- Index289
Inductively Coupled Plasma-Mass Spectrometry presents a concise A-Z description of inductively coupled plasma-mass spectrometry, written in layman's terms, for use in the solution of trace element analytical chemistry problems. Detailed discussion of sample introduction and data interpretation is provided.
Practicing analytical chemists will be able to use this text to familiarize themselves with the principles, approaches, options, pitfalls, and advantages of ICP-MS technology.
Key Features
* Concise and straightforward descriptions of ICP-MS principles and instrumentation, ensuring rapid understanding of the technique and its advantages and limitations
* Examples to clarify the operational characteristics of the technology
* Drawings and illustrations to clarify principles, techniques, and methodology
* Discussions of practical approaches to the solution of specific trace analysis problems with helpful tips on efficiently producing the most accurate and precise data
* Easy-to-understand terms, so that new users of the technology will immediately benefit from the information provided
* Comprehensive appendixes containing isotopic and interference data
* An exhaustive compilation of literature citations for supplemental information
Practicing analytical chemists will be able to use this text to familiarize themselves with the principles, approaches, options, pitfalls, and advantages of ICP-MS technology.
Key Features
* Concise and straightforward descriptions of ICP-MS principles and instrumentation, ensuring rapid understanding of the technique and its advantages and limitations
* Examples to clarify the operational characteristics of the technology
* Drawings and illustrations to clarify principles, techniques, and methodology
* Discussions of practical approaches to the solution of specific trace analysis problems with helpful tips on efficiently producing the most accurate and precise data
* Easy-to-understand terms, so that new users of the technology will immediately benefit from the information provided
* Comprehensive appendixes containing isotopic and interference data
* An exhaustive compilation of literature citations for supplemental information