Elsevier S & T

Nanoporous Materials III

Jaroniec, M.; Sayari, Abdel

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Table of contents

Cover
CONTENTSix
Prefacev
Organizing Committeevii
Intemational Advisory Committeevii
Section I: Plenary Lectures1
Chapter 1. Recent Developments in the Synthesis and Chemistry of Periodic Mesoporous Organosilicas1
Chapter 2. Porous Materials: Looking Through the Electron Microscope27
Chapter 3. Molecular Imprinting - A Way to Prepare Effective Mimics of Natural Antibodies and Enzyme35
Section II: Synthesis of Mesoporous Silicas45
Chapter 4. Plugged Hexagonal Mesoporous Templated Silica: A Unique Micro- and Mesoporous Material wi45
Chapter 5. Imprinting of the Surface of Mesoporous Silicates using Organic Structure Directing Agent53
Chapter 6. Synthesis and Characterization of Polymer-Templated Ordered Silica with Cage-like Mesostr61
Chapter 7. The Modeling of Wall Structure of Siliceous MCM-41 Based on the Formation Process69
Chapter 8. Pore Size Adjustment of Bimodal-mesoporous Silica Molecular Sieves77
Chapter 9. Alcothermal Synthesis of Large Pore, High Quality MCM-48 Silica85
Chapter 10. Studies of MCM-41 Obtained from Different Sources of Silica93
Chapter 11. Synthesis and Characterization of Hexagonal Mesoporous Materials Using Hydrothermal Rest101
Chapter 12. Synthesis of Highly Ordered Mesoporous Compounds with Control of Morphology Using a Non-101
Chapter 13. Towards a Better Understanding on the Mechanism of Mesoporous Formation via an Assembly117
Chapter 14. Mesoporous Silicas via Organic-Inorganic Hybrids Based on Charged Polymers127
Chapter 15. Mesoporous Silicas of Hierarchical Structure by Hydrothermal Surfactant-Templating under133
Section III: Synthesis of Framework-Modified Mesoporous Silicas141
Chapter 16. Synthesis and Characterisation of Super-microporous Aluminosilicates Prepared via Primar141
Chapter 17. A1-MCM-41 Synthesis Studies Using Al-Isopropoxide as A1 Source151
Chapter 18. Mesoporous Aluminosilicates from Coal Fly Ash159
Chapter 19. New Route for Synthesis of Highly Ordered Mesoporous Silica with Very High Titanium Cont167
Chapter 20. Synthesis and Characterization of Ti-containing Mesoporous Alumina Molecular Sieves173
Section IV: Synthesis of Surface-Modified Mesoporous Silicas183
Chapter 21. Organizing One-Dimensional Molecular Wires in Ordered Mesoporous Silica183
Chapter 22. Synthesis and Catalytic Properties of Organically Modified Ti-HMS189
Chapter 23. Synthesis and Characterization of Methyl- and Vinyl-Functionalized Ordered Mesoporous Si197
Chapter 24. Polyfunctionalized Silica Adsorbents Obtained by Using Dodecylamine as Template Jaroniec205
Chapter 25. Characterization of Mesoporous Thin Films Formed with Added Organophosphonate and Organo213
Chapter 26. Improving the Hydro-Stability of MCM-41 by Post-Synthesis Treatment and Hexamethyldisila221
Chapter 27. Adsorption of CO on Zn-Cu(I)/HMCM-41229
Section V: Synthesis of Mesoporous Metal Oxides235
Chapter 28. Design of Transition Metal Oxide Mesoporous Thin Films235
Chapter 29. Mesoporous Alumina as A Support for Hydrodesulphurization Catalysts243
Chapter 30. Preparation and XAFS Spectroscopic Characterization of Mesoporous Titania with Surface A251
Chapter 31. Mesoporous Zirconium Oxides: An Investigation of Physico-chemical Synthesis Parameters257
Chapter 32. Single Crystal Particles of Mesoporous (Nb, Ta)2O5265
Section VI: Synthesis of Other Nanostructured Materials and Nanoparticles273
Chapter 33. Preparation of Exfoliated Zeolites from Layered Precursors - The Role of pH and Nature o273
Chapter 34. Control of Mesopore Structure of Smectite-type Materials Synthesized with a Hydrothermal281
Chapter 35. Synthesis, Characterization and Catalytic Application of Mesoporous Sulfated Zirconia289
Chapter 36. Synthesis of Mesoporous Silicoaluminophosphates (SAPO)297
Chapter 37. Synthesis and Characterization of Mesostructured Vanadium-Phosphorus-Oxide Phases301
Chapter 38. Novel Macroporous Vanadium-Phosphorus-Oxides with Three-Dimensional Arrays of Spherical309
Chapter 39. Engineering Active Sites in Bifunctional Nanopore and Bimetallic Nanoparticle Catalystsf317
Chapter 40. Using Au Nanoparticles-Surfactant Aqueous Solution for a Convenient Preparation of Mesop329
Chapter 41. The Use of Templated Mesoporous Materials as Tempates for the Development of Odered Arra337
Chapter 42. Synthesis and Adsorption Properties of Novel Carbons of Tailored Porosity345
Chapter 43. Flexible Metal-Organic Frameworks with Isomerizing Building Units353
Chapter 44. Dynamic Porous Frameworks of Coordination Polymers Controlled by Anions363
Chapter 45. Mesoporous Polymeric Materials Based On Comb-Coil Supramolecules371
Section VII: Characterization of Nanoporous Materials379
Chapter 46. Electron Microscopic Investigation of Mesoporous SBA-2379
Chapter 47. A Study of Morphology of Mesoporous Silica SBA-15387
Chapter 48. SBA- 15 versus MCM-41: Are they the same Materials?395
Chapter 49. Comprehensive Characterization of Iron Oxide Containing Mesoporous Molecular Sieve MCM-4403
Chapter 50. Mesoporous Molecular Sieves of MCM-41 Type Modified with Cs, K and Mg -Physico-Chemica l411
Chapter 51. Meso-ALPO Prepared by Thermal Decomposition of the Organic-Inorganic Composite. A FTIR S417
Chapter 52. Organic - Inorganic Phase Interaction in A1SBA-15 Mesoporous Molecular Sieves by DoubleR423
Chapter 53. Adsorption of Nitrogen on Organized Mesoporous Alumina429
Chapter 54. The Use of Ordered Mesoporous Materials for Improving the Mesopore Size Analysis: Curren437
Chapter 55. Sorption Properties and Hydrothermal Stability of MCM-41 Prepared by pH Adjustment and S445
Chapter 56. Acidity Characterization of MCM-41 Materials Using Solid-State NMR Spectroscopy453
Chapter 57. Acidity of Calcined AI-, Fe-, and La-containing MCM-41 Mesoporous Materials: An Investig459
Chapter 58. Acid Properties of Ammonium Exchanged A1MCM-41 with Different Si/A1 Ratio467
Chapter 59. Kinetic Evaluation of the Pyrolysis of High Density Polyethylene over H- A1MCM-41 Materi473
Chapter 60. Electrorheological Response of Mesoporous Materials under Applied Electric Fields479
Section VIII: Catalytic Applications of Nanoporous Materials487
Chapter 61. Synthesis and Characterization of TiO2 Loaded Cr-MCM-41 catalysts487
Chapter 62. Photocatalytic Ethylene Polymerization over Chromium Containing Mesoporous Molecular Sie495
Chapter 63. Catalytic Reduction of Nitric Oxides on A1- containing Mesoporous Molecular Sieves503
Chapter 64. Catalytic Oxidation of alpha-Eicosanol to alpha-Eicosanoic Acid Over Ti, Zr and Mn Doped511
Chapter 65. Preparation of Pd/A1-MCM-41 Catalyst and Its Hydroisomerization Properties for Long Chai517
Chapter 66. Isopropanol Dehydration over Nanostructured Sulfated MCM-41531
Chapter 67. Effect of Si/A1 Ratio and Pore Size on Cracking Reaction over Mesoporous MCM-41537
Chapter 68. Hydrogenation and Mild Hydrocracking of Synthetic Crude Distillate by Pt-supported Mesop543
Chapter 69. Carbon-Carbon Bond Forming Reactions Catalyzed by Meso- and Microporous Silicate-Quatern553
Chapter 70. A Selectivity of Zeolite Matrices in the Cu(II) Reduction Process561
Chapter 71. Reduction of Binary Silver-Copper Ion Mixture in Mordenite: an Example of Synergetic Beh569
Chapter 72. Preparation, Characterization and Catalytic Properties of CuPC/Y Nano-composite575
Section IX: Environmental Applications of Nanoporous Materials583
Chapter 73. Environmental Applications of Self-Assembled Monolayers on Mesoporous Supports (SAMMS)583
Chapter 74. A Possible Use of Modified Mesoporous Molecular Sieves in Water Treatment Processes591
Chapter 75. Organized Mesoporous Titanium Dioxide - A Powerful Photocatalyst for the Removal of Wate599
Chapter 76. Mesoporous Materials for Heavy Metal Ion Adsorption Synthesized by Displacement of Polym607
Chapter 77. Organically-modified Mesoporous Silica Spheres with MCM-41 Architecture as Sorbents for615
Chapter 78. NO and NO2 Gas Sensors Based on Surface Photovoltage System are Fabricated by Self-order623
Section X: Other Applications of Nanoporous Materials631
Chapter 79. Polymerisations in Mesoporous Environments631
Chapter 80. Incorporation of Nano-sized zeolites into a Mesoporous Matrix, TUD-1635
Chapter 81. Formation and Stabilization of Gold Nanoparticles in Organo-Functionalized MCM-41 Mesopo641
Chapter 82. Entrapment and Stabilization of Cadmium Sulphide (CdS) Nanoclusters Formed Inside Propyl647
Chapter 83. SnO2 Nanoparticles in the Pores of Non-structured SiO2 and of Si-MCM-41: Comparison of t653
Chapter 84. Spontaneous Nitride Formation in the Reaction of Mesoporous Titanium Oxide with Bis(Tolu661
Chapter 85. Isolation and Characterization of Amorphous Solids from Oil Sands Fine Tailings669
Author Index675
Subject Index679

Book details

Vendor Elsevier S & T
SKU 9780444511133
ISBN-13 9780080537221
Author Jaroniec, M.; Sayari, Abdel
Category Technology & Engineering
Subject Materials Science

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Nanoporous Materials III contains the invited lectures and peer-reviewed oral and poster contributions to be presented at the 3rd Conference on Nanoporous Materials, which will be hosted in Ottawa, Canada, June 2002. The work covers complementary approaches to and recent advances in the field of nanostructured materials with pore sizes larger than 1nm, such as periodic mesoporous molecular sieves M41S and FSM16 and related materials including clays, carbon molecular sieves, colloidal crystal templated organic and inorganic materials, porous polymers and sol gels. The broad range of topics covered in relation to the synthesis and characterization of ordered mesoporous materials are of great importance for advanced adsorption, catalytic and separation processes as well as the development of nanotechnology.

The contents of this title are based on topics to be discussed by invited lecturers, which deal with periodic mesoporous organosilicas, stability and catalytic activity of aluminosilicate mesostructures, electron microscopy studies of ordered materials, imprinted polymers and highly porous metal-organic frameworks. The other contributions deal with tailoring the surface and structural properties of nanoporous materials, giving a detailed characterization as well as demonstrating their usefulness for advanced adsorption and catalytic applications.

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