Elsevier S & T

Nanotechnology in Mesostructured Materials: Proceedings of the 3rd International Mesostructured Materials Symposium, Jeju, Korea, July 8-11, 2002

Park, Sang-Eon; Ryoo, Ryong; Ahn, Wha-Seung; Lee, Chul Wee; Chang

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Table of contents

Cover
Contentsv
Prefacexix
Organizing committeexxi
International advisory boardxxii
Local advisory boardxxii
Supporting organizationsxxiii
Financial supportxxiii
Part I: Synthesis and materials1
Chapter 1. A new family of organic-bridged mesoporous materials1
Chapter 2. Strategies to fabricate large-pore three-dimensional mesoporous materials with versatile9
Chapter 3. Mesostructured solid acids15
Chapter 4. Template synthesis and catalysis of metal nanowires in mesoporous silicas23
Chapter 5. Mesostructured silica films with crystalline domains and structural features on multiple29
Chapter 6. Synthesis of mesoporous carbons with various pore diameters via control of pore wall thic33
Chapter 7. Ordered mesoporous carbon molecular sieves with functionalized surfaces37
Chapter 8. Characterisation of ordered mesoporous carbons and their MCM-48 silica templates obtained41
Chapter 9. Morphological control of highly ordered mesoporous carbon45
Chapter 10. Thermally induced structural changes in SBA-15 and MSU-H silicas and their implications49
Chapter 11. Regeneration of mesoporous inorganic materials using ordered mesoporous carbon as the te53
Chapter 12. A novel preparation route for palladium-carbon composite materials - pore filling of SBA57
Chapter 13. Structure of ultra-thin RbBr "Solution" in carbon nanospace61
Chapter 14. Synthesis and characterization of mesoporous silica films by spin-coating on silicon: ph65
Chapter 15. Synthesis of 2D hexagonal mesoporous silica thin films via phase transition from lamella69
Chapter 16. Nanostructured silicate film templated by discotic CT-complex column73
Chapter 17. Mesoporous titania thin film with cubic mesostructure using photocalcination77
Chapter 18. Preparation of tin modified silica mesoporous film81
Chapter 19. Novel non-lithographic large area fabrication method to generate various polymeric nanos85
Chapter 20. Mesoporous anodic alumina mbembrane with highly ordered arrays of uniform nanohole89
Chapter 21. Preparation and characterization of poly(ester)-silver and nylon-silver nanocomposites93
Chapter 22. Synthesis of ordered three-dimensional large-pore mesoporous silica and its replication97
Chapter 23. Morphology control of mesoporous SBA-16 using microwave irradiation101
Chapter 24. One-Step synthesis of mesoporous silica SBA-15 with ultra-high microporosity105
Chapter 25. Controlling the pore sizes of SBA-15 mesoporous silica by the addition of poly(propylene109
Chapter 26. Synthesis of mesoporous silicas with different pore size by using EOmMAn diblock copolym113
Chapter 27. Polypropylene glycol as a swelling agent for the synthesis of mesoporous silica (SBA-15)117
Chapter 28. Thermal decomposition-precipitation inside the nanoreactors high loading of W-oxide nano121
Chapter 29. Phase transition of SBA-1 induced by embedded heteropoly acids125
Chapter 30. A further investigation on effect of basic media on the synthesis of MCM-41129
Chapter 31. Cationic templating with organic counterion for superstable mesoporous silica133
Chapter 32. The synthesis of mesoporous materials with semicrystalline microporous walls137
Chapter 33. Synthesis of a mesoporous molecular sieve with hydrothermal stability141
Chapter 34. Diffusive characterization of large pore mesoporous materials with semi-crystalline zeol145
Chapter 35. Synthesis of cubic mesoporous aluminosilicates with enhanced acidity149
Chapter 36. Synthesis and characterization of supersurface MCM-41 zeolite using additives153
Chapter 37. Preparation of large pore high quality MCM-48 silica by a simple post-synthesis hydrothe157
Chapter 38. Synthesis and properties of aluminosilicate mesoporous material with adjustable pore str161
Chapter 39. Variation of the pore properties of mesoporous silica after washing by water and ethanol165
Chapter 40. Sythesis of ordered lamella mesophase from helix layered silicate (HLS)169
Chapter 41. Sythesis of monolithic nanostructured silicate family materials through the lyotropic li173
Chapter 42. Synthesis and characterization of a new mesoporous molecular sieve177
Chapter 43. Direct- and post-hydrothermal treatments in ammoniated solution for the morphogenesis of181
Chapter 44. Generalized homogeneous precipitation method for precisely controlled synthesis of mesop185
Chapter 45. Synthesis of mesoporous silica particles preapared by using multiple emulsion189
Chapter 46. Preparation and characterization of mesoporous silica spheres by polymerization induced197
Chapter 47. Preparation of mesoporous solids by agglomeration of silica nanospheres197
Chapter 48. Ordered mesostructured materials with composite walls of decavanadate and silica201
Chapter 49. Nanoporous alumina formation using mulit-step anodization and cathodic electrodeposition205
Chapter 50. Synthesis of mesoporous γ-aluminas of controlled pore properties using alkyl carboxylat209
Chapter 51. Synthesis and characterization of mesoporous alumina molecular sieves using cationic sur213
Chapter 52. Synthesis and characterization of mesoporous alumina molecular sieves with cationic surf217
Chapter 53. Structure and properties of porous mesostructured zirconium oxo-phosphate with cubic(Ia-221
Chapter 54. Synthesis and characterization of mesoporous titanium oxide227
Chapter 55. Improvement of thermal stability of Ti-Zr mesoporous oxides using CTAB surfactant templa231
Chapter 56. Synthesis and characterization of mesoporous zirconia235
Chapter 57. A novel method to prepare mesoporous nano-zirconia239
Chapter 58. Control of ordered mesoporous molecular sieves synthesis using non-ionic surfactants by243
Chapter 59. Texture of chromia aerogels and structure of their nanocrystals247
Chapter 60. Preparation of ordered mesoporous NbTa mixed oxide with crystallized wall251
Chapter 61. Compositional effects of bimodal mesopore silica synthesized by a base-catalyzed ambient255
Chapter 62. A direct template synthesis of highly ordered mesostructured carbons using as-synthesize259
Part II: Characterization263
Chapter 63. Gas adsorption: a valuable tool for the pore size analysis and pore structure elucidatio263
Chapter 64. Three-dimensional transmission electron microscopy of disordered and ordered mesoporous271
Chapter 65. Structures of silica-mesoporous crystals and novel mesoporous carbon-networks synthesize275
Chapter 66. Phase transformations involved during silica, modified silica, and non-silica mesoporous281
Chapter 67. Comparison of the mechanical stability of cubic and hexagonal mesoporous molecular sieve285
Chapter 68. Fs-time-resolved diffuse reflectance and resonance Raman spectroscopic studies on MCM-41289
Chapter 69. Detailed investigation of the microporous character of mesoporous silicas as revealed by295
Chapter 70. X-ray diffraction analysis of mesostructured materials by continuous density function te299
Chapter 71. Influence of aluminium, lanthanum and cerium on the thermal and hydrothermal stability o303
Chapter 72. Enhanced acidity and hydrothermal stability of mesoporous aluminosilicate with secondary307
Chapter 73. Chemical coating of the aluminum oxides onto mesoporous silicas by a one-pot grafting me311
Chapter 74. Acidity and temperature effect on the synthesis of SBA-1315
Chapter 75. HMS materials with high Al loading: a joint FT-IR and microcalorimetric study of their a319
Chapter 76. Effect of cations addition for the highly ordered mesoporous niobium oxide323
Chapter 77. Synthesis of zirconium-containing mesoporous silica Zr-MCM-48 membranes with high alkali327
Chapter 78. Synthesis of siliceous MCM-41 grafted with transition metal carbonyls331
Chapter 79. Surface and pore structures of CMK-5 ordered mesoporous carbons studied by nitrogen adso335
Chapter 80. A comparison of the sorption properties of mesoporous molecular sieves MCM-41 and MCM-48339
Chapter 81. Argon and nitrogen adsorption on ordered silicas with channel-like and cage-like mesopor343
Chapter 82. Mesopores developed in KL zeolite dealuminated with (NH4)2SiF6 solution347
Chapter 83. Time-resolved in situ grazing incidence small angle x-ray scattering experiment of evapo351
Chapter 84. Small angle neutron scattering study on the formation mechanism of mesostructures during355
Chapter 85. Preparation of mesoporous silica anchored Mo catalysts and in-situ XAFS characterization359
Chapter 86. In-situ XAFS observation of formation of Pd-Pt bimetallic particles in a mesoporous USY363
Chapter 87. Investigation of the internal pore structures of Beta/MCM-41 and ZSM-5/MCM-41 composites367
Chapter 88. Study of chromium species in the Cr-MCM-48 mesoporous materials by Raman spectroscopy371
Chapter 89. Covalent bonding of Disperse Red 1 in HMS silica: synthesis and characterization375
Chapter 90. Accessibility of dye-molecules embedded in the micellar phase of hybrid mesostructured M379
Chapter 91. Influence of surface properties of MCM-48 on the formation of a nanocomposite structure383
Chapter 92. A study on the structure of Si-O-C thin films with nano size pore by ICPCVD387
Chapter 93. Template effects on low k materials made from spin-on mesoporous silica391
Chapter 94. Porosity tuning of single-wall carbon nanohoms with gaseous activation395
Part III: Modification and composite399
Chapter 95. Expanding horizons of mesoporous materials to non-siliceous systems399
Chapter 96. Structure and shape control in functional mesostructured materials from block copolymer407
Chapter 97. Strategies for spatially separating photoactive molecules in mesostructured sol-gel sili413
Chapter 98. Design of supported catalysts by surface functionalization of micelle-templated silicas419
Chapter 99. Proteosilica-mesoporous silicates densely filling amino acid and peptide assemblies in t427
Chapter 100. Counteranion effect on the formation of mesoporous materials under acidic synthesis pro431
Chapter 101. Influence of alumination pathway on the steam stability of Al-grafted MCM-41435
Chapter 102. Macroporous titanium oxides: from highly aggregated to isolated hollow spheres439
Chapter 103. Nanostructured mesoporous TiO2, ZrO2 and SiO2 synthesis by using the non-ionic Cm(EO)n443
Chapter 104. Morphology control of hierarchically ordered ceramic materials prepared by surfactant-d447
Chapter 105. A NH3-responding material based on Reichardt's dye-impregnated mesoporous silica453
Chapter 106. Preparation and redox behavior of ordered porous zirconium oxide loaded with cerium457
Chapter 107. Direct synthesis of bi-fimctionalized organo-MSU-X silicas461
Chapter 108. High-density modification of mesoporous silica inner walls with amino acid function by465
Chapter 109. The synthesis of optically active amino acid over Pd catalysts impregnated on mesoporou469
Chapter 110. Sulfonic acid-functionalized periodic mesoprous organosilicas473
Chapter 111. Functionalized periodic mesoporous organosilicas with sulfonic acid group477
Chapter 112. Exclusive incorporation of aluminum into tetrahedral site of the framework of periodic481
Chapter 113. Functionalization of hexagonal mesoporous silica and their base-catalytic performance485
Chapter 114. Microstructure of the organo-modified SBA-15 (Vinyl-SBA 15) prepared under different pH489
Chapter 115. Surface coating of MCM-48 via a gas phase reaction with hexamethyldisilazane (HMDS)493
Chapter 116. Reacitvity of silica walls of mesoporous materials towards benzoyl chloride497
Chapter 117. Catalytic activitiy of chiral phosphinooxazolidine ligands immobilized on SBA-15 for th501
Chapter 118. Preparation of guanidine bases immobilized on SBA-15 mesoporous material and their cata505
Chapter 119. MCM-41-supported norephedrine ligand for ruthenium-catalyzed asymmetric transfer hydrog509
Chapter 120. Synthesis of silica support for biocatalyst immobilization513
Chapter 121. Mesostructured materials for controlled macromolecular and supramolecular architectures517
Chapter 122. Nanocomposites of MCM-41 and SBA-15 with polyaniline for electrorheological fluid523
Chapter 123. Functionalized mesoporous adsorbents for Pt(II) and Pd(II) adsorption from dilute aqueo527
Chapter 124. Environmentally benign removal of pollutant oxyanions by Fe adsorption center in functi531
Chapter 125. How can nanoparticles change the mechanical resistance of ordered mesoporous thin films535
Chapter 126. Nanoporous SiO2 films prepared by surfactant templating method - a novel antireflective539
Chapter 127. Textural and structural properties of Al-SBA-15 directly synthesized at 2.9 < pH < 3.3543
Chapter 128. Fabrication of nanostructured SiC and BN from templated preceramic polymers547
Part IV: Application and catalysis551
Chapter 129. Mesoporous solids for green chemistry551
Chapter 130. Ultrastable acidic MCM-48-S assembled from zeolite seeds557
Chapter 131. Acidic zeolite coated mesoporous aluminosilicates561
Chapter 132. Stable ordered mesoporous titanosilicates with active catalytic sites565
Chapter 133. W/Zr mixed oxide supported on mesoporous silica as catalyst for n-pentane isomerization569
Chapter 134. Au and Au-Pt bimetallic nanoparticles in MCM-41 materials: applications in CO preferent573
Chapter 135. Effective inclusion of chlorophyllous pigments into mesoporous silica for the energy tr577
Chapter 136. Biological applications of organically functionalised mesoporous molecular sieves and r581
Chapter 137. One pot synthesis of mesoporous ternary V2O5-TiO2-SiO2 catalysts585
Chapter 138. Photocatalytic hydroxylation of benzene on Ti-modified MCM-41 with both framework and n589
Chapter 139. The relationship between the local structures and photocatalytic reactivity of Ti-MCM-4593
Chapter 140. Photocatalytic epoxidation of propene with molecular oxygen under visible light irradia597
Chapter 141. Mesostructured TiO2 films as effective photocatalysts for the degradation of organic po601
Chapter 142. Comparisons of the structural and catalytic properties of Ti-HMS synthesized using the605
Chapter 143. Oxidation of methyl-propyl-thioether with hydrogen peroxide using Ti-SBA-15 as catalyst609
Chapter 144. Direct synthesis of hydrothermally stable mesoporous Ti-MSU-G and its catalytic propert613
Chapter 145. Mesoporous V-containing MCM-41 molecular sieves: synthesis, characterization and cataly617
Chapter 146. Catalytic oxidation of H2S to elemental sulfur over mesoporous Nb/Fe mixed oxides621
Chapter 147. Fe-MCM-41 catalyzed epoxidation of alkenes with hydrogen peroxide625
Chapter 148. Highly selective oxidation of styrene with hydrogen peroxide catalyzed by mono- and bim629
Chapter 149. Mixed (Al-Cu) pillared clays as wet peroxide oxidation catalysts633
Chapter 150. Finely-dispersed Ni/Cu catalysts supported on mesoporous silica for the hydrodechlorina637
Chapter 151. New SO2 resistant mesoporous mixed oxide catalysts for methane oxidation641
Chapter 152. Decomposition of VOCs using mesoporous TiO2 in a silent plasma645
Chapter 153. Preparation of mesoporous 12-tungstophosphoric acid HPW/Si02 and its catalytic performa649
Chapter 154. Catalytic properties of heteropolyacids supported on MCM-41 mesoporous silica for hydro653
Chapter 155. Preparation, characterization and catalytic activity of heteropolyacids supported on me657
Chapter 156. Novel SBA-15 supported heteropoly acid catalysts for benzene alkylation with 1-dodecene661
Chapter 157. Aluminum containing periodic mesoporous organosilicas: synthesis and etherification665
Chapter 158. Friedel-crafts alkylation over Al-incorporated mesoporous honeycomb669
Chapter 159. Heterogenization of AICI3 on mesoporous molecular sieves and its catalytic activity673
Chapter 160. Asymmetric dihydroxylation catalyzed by MCM-41 silica-supported bis-cinchona alkaloid677
Chapter 161. Roles of pore size and Al content on the catalytic performance of Al-MCM-41 during hydr681
Chapter 162. HDS of FCC gasoline: Mesoporous modified support catalyst and its effects on the hydrog685
Chapter 163. Synthesis of mesoporous carbon nanotubes and their application in gas phase benzene hyd689
Chapter 164. Characteristics and reactivities of cobalt based mesoporous silica catalysts for Fische693
Chapter 165. Physicochemical characteristics of Ti-PILC as a catalyst support for the reduction of N697
Chapter 166. Performance of double wash-coated monolith catalyst in selective catalytic reduction of701
Chapter 167. Copper loaded MCM-41. An alternative catalyst for NO reduction in exhaust gases ? - Stu705
Chapter 168. Studies on synthesis and activity for selective catalytic reduction of NO over Pt suppo709
Chapter 169. Synthesis of titania-pillared clays and their application as catalyst supports for sele713
Chapter 170. Hydrogenation of aromatics on Pt/Pd bimetallic catalyst supported by Al-containing meso717
Chapter 171. High loading of short W(Mo)S2 slabs inside the nanotubes of SBA-15. Promotion with Ni(C721
Chapter 172. Cr-MCM-41 for selective dehydrogenation of lower alkanes with carbon dioxide725
Chapter 173. Methane reforming on molybdenum carbide on Al-FSM-16729
Chapter 174. Preparation of carbided WO3/FSM-16 and Al-FSM-16 and its catalytic activity733
Chapter 175. AMI study on the catalytical isomerization of 1-hexene to 2-hexene on the surface of al737
Chapter 176. Isomerization and hydrocracking of n-decane over Pt/MCM-41//MgAPO-n composite catalysts741
Chapter 177. Catalytic properties of mesoporous aluminosilicates and lanthanum containing mesoporous745
Chapter 178. Diels-Alder reaction catalyzed by ordered micro- and mesoporous silicates749
Chapter 179. Isospecific polymerization of propylene with metal-MCM-41753
Chapter 180. A possibility of block-copolymer templated mesoporous silica films applied to surface p783
Chapter 181. Proton conducting silica mesoporous/heteropolyacid-PVA/SSA nano-composite membrance for787
Chapter 182. Hydrothermal synthesis of titania nanotube and its application for dye- sensitized sola791
Chapter 183. Preparation of hydrophobic Ti-containing mesoporous silica by the F-modification and th795
Chapter 184. Synthesis of functionalised silicas for immobilisation of homogeneous catalysts799
Author index803
Subject index811
Other volumes in the series815

Book details

Vendor Elsevier S & T
SKU 9780444514349
ISBN-13 9780080537283
Author Park, Sang-Eon; Ryoo, Ryong; Ahn, Wha-Seung; Lee, Chul Wee; Chang
Category Technology & Engineering
Subject Chemical & Biochemical

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In these proceedings the reader will find regular papers from many groups worldwide, covering the most recent advances in mesostructured materials and providing future perspectives of nanotechnology.

Presents the Proceedings of the 3rd International Mesostructured Materials Symposium
Discusses the most recent advances in synthesis characterization, and applications of mesostructured materials

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