Elsevier S & T

Scientific Bases for the Preparation of Heterogeneous Catalysts: Proceedings of the 9th International Symposium Louvain-la-Neuve, Belgium, September 10-14, 2006

Gaigneaux*, E.; Devillers, M; De Vos**, D.E.; Hermans, S.; Jacobs, P.; Martens, J.; Ruiz, P.

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Table of contents
  • Front CoverCover
  • Scientific Bases For The Preparation of Heterogeneous Catalystsiii
  • Copyright Pageiv
  • Forewordv
  • Table of Contentsxi
  • Scopes and limitations of high throughput preparation and screening tools1
  • 1. Introduction1
  • 2. HTE definition, targets, workflow2
  • 3. HTE techniques4
  • 4. HTE and knowledge generation6
  • 5. HTE and Up-Scaling Process6
  • 6. Conclusions11
  • References11
  • Mesoporous alumina of controlled pore size obtained by surface alumination of pure silica SBA-1513
  • Abstract13
  • 1. Introduction13
  • 2. Experimental Section14
  • 3. Results and discussion16
  • 4. Conclusion20
  • References20
  • Biomimetic catalyst preparation with carbohydrates: The Carbohydrate-Sol-Gel (CHSG) process21
  • 1. Introduction21
  • 2. Experimental section22
  • 3. Results24
  • Acknowledgements28
  • References28
  • Synthesis of heterogeneous base catalyst: nitrogen containing carbon nanotubes29
  • abstract29
  • 1. Introduction29
  • 2. Experimental30
  • 3. Characterization31
  • 4. Results and discussion31
  • 5. Conclusion35
  • Acknowledgements36
  • References36
  • Tooling up heterogeneous catalysis through Fenton's chemistry. Detemplation and functionalization of37
  • 1. Background37
  • 2. Experimental38
  • 3. Results and discussion40
  • 4. Conclusions46
  • 5. Literature46
  • Molybdenum and tungsten carbides supported on mesostructured MCM-41 materials with polymeric carbon47
  • 1. Introduction47
  • 2. Experimental48
  • 3. Results and discussion48
  • 4. Conclusions54
  • 5. References54
  • Comparison of microwave and hydrothermal approaches to the synthesis of tin-containing mesoporous mo55
  • 1. Introduction55
  • 2. Experimental56
  • 3. Results and discussion57
  • 4. Conclusions61
  • Acknowledgement62
  • References62
  • Preparation of hollow silica-Rh, -Ir and -Rh-lr-bimetallic nanocomposites by reverse micelle techniq63
  • 1. Introduction63
  • 2. Experimental64
  • 3. Results and discussion65
  • 4. Conclusion69
  • 5. References70
  • The use of magnetron sputtering for the production of heterogeneous catalysts71
  • 1. Introduction71
  • 2. Experimental Procedure72
  • 3. Results and Discussion74
  • 4. Conclusion77
  • 5. Acknowledgements77
  • References78
  • Preparation of carbon-supported Pd and Au-Pd catalysts via optimized adsorption of metallic complexe79
  • Abstract79
  • 1. Introduction79
  • 2. Experimental80
  • 3. Results and discussion82
  • 4. Conclusion86
  • 5. References86
  • Supported Ionic Liquid Catalyst (SILCA) in the hydrogenation of citral87
  • 1. Introduction87
  • 2. Experimental88
  • 3. Results and discussion89
  • 4. Conclusions93
  • References94
  • Application of ordered mesoporous materials as model supports to study catalyst preparation by impre95
  • 1. Introduction95
  • 2. Experimental97
  • 3. Results and discussion98
  • 4. Conclusions101
  • Acknowledgements102
  • References102
  • Supported metal catalysts: some interesting new leads in an old field103
  • 1. Abstract103
  • 2. Introduction103
  • 3. Experimental104
  • 4. Results and discussion106
  • 5. Conclusion109
  • 6. Acknowlegments110
  • References110
  • Metal catalysts supported on texture tailored carbon xerogels111
  • Abstract111
  • 1. Introduction111
  • 2. Experimental112
  • 3. Results and discussion113
  • 4. Conclusion118
  • References118
  • Novel nano catalysts on the base of hypercrosslinked polystyrene for carbohydrates oxidation119
  • 1. Introduction119
  • 2. Experimental120
  • 3. Results and Discussions122
  • 4. Conclusions126
  • Acknowledgements126
  • References126
  • Effect of the titania morphology on the preparation of Au/TiO2(/SiO2) catalysts127
  • Abstract127
  • 1. Introduction127
  • 2. Experimental128
  • 3. Results and discussion130
  • 4. Conclusion134
  • References134
  • Structured ceramic foams as catalyst supports for highly exothermic processes135
  • 1. Introduction135
  • 2. Experimental137
  • 3. Results and discussion138
  • 4. Conclusions141
  • 5. Acknowledgments142
  • References142
  • Preparation of monolithic catalysts for hydrodesulfurization143
  • 1. Abstract143
  • 2. Introduction143
  • 3. Experimental144
  • 4. Results and Discussion147
  • 5. Conclusions150
  • 6. Acknowledgments150
  • 7. References150
  • Structured TiO2 based catalysts for clean water technologies151
  • 1. Abstract151
  • 2. Introduction151
  • 3. Experimental152
  • 4. Results and discussion154
  • 5. Conclusions158
  • Acknowledgments158
  • References158
  • Single-step synthesis of porous supported catalysts159
  • 1. Introduction159
  • 2. Experimental160
  • 3. Results and discussion162
  • 4. Conclusions165
  • References165
  • Preparation and characterization of bimetallic catalysts supported on mesoporous silica films167
  • 1. Introduction168
  • 2. Experimental169
  • 3. Results and discussion171
  • 4. Conclusions173
  • 5. Acknowledgements173
  • 6. References174
  • Monitoring the preparation of (Co)Mo/AI2O3 extrudates using spatially resolved spectroscopic techniq175
  • 1. Introduction175
  • 2. Raman spectroscopy177
  • 3. UV-Vis spectroscopy179
  • 4. Magnetic Resonance Imaging183
  • 5. Conclusions185
  • Acknowledgments185
  • References186
  • Parameters controlling the scaling-up of a V-AI oxynitride catalyst for the ammoxidation of propane187
  • Abstract187
  • 1. Introduction187
  • 2. Experimental188
  • 3. Results and discussion191
  • 4. Conclusions193
  • 5. Acknowledgements194
  • 6. References194
  • Approaching the preparation of Pd-Al2O3 catalyst systematically: one step closer to reproducible cat195
  • Abstract195
  • 1. Introduction195
  • 2. Methodology and Experimental196
  • 3. Results and discussion199
  • 4. Conclusion and perspectives201
  • Acknowledgments202
  • References202
  • Design and preparation of controlled porous oxidic structures on metallic substrates203
  • Abstract203
  • 1. Introduction and motivation203
  • 2. Experimental204
  • 3. Results and discussion205
  • 4. Conclusion210
  • References210
  • Simple, scientific syntheses with common catalyst precursors211
  • Abstract211
  • Introduction211
  • Strong Electrostatic Adsorption212
  • Experimental213
  • Results and Discussion213
  • Conclusions218
  • Acknowledgements218
  • References218
  • Preparation of TiO2 using supercritical CO2 antisolvent precipitation (SAS): A support for high acti219
  • Abstract219
  • 1. Introduction219
  • 2. Experimental220
  • 3. Results and Discussion222
  • 4. Conclusion225
  • References225
  • Clean transesterification of Beta-ketoesters catalyzed by hybrid silica sol-gel227
  • Abstract227
  • 1. Introduction227
  • 2. Experimental228
  • 3. Results and Discussion229
  • 4. Conclusion234
  • 5. References234
  • Development of tools and methods for the high-throughput preparation of commercial heterogeneous cat235
  • 1. Abstract235
  • 2. Introduction235
  • 3. High-Throughput Experimentation for Industrial Purposes236
  • 4. Results239
  • 5. Conclusions242
  • 6. Acknowledgment242
  • References242
  • Production of catalysts with an inductive atmospheric plasma torch243
  • Abstract243
  • Introduction243
  • Experimental244
  • Conclusions250
  • References250
  • Investigation of the mode of interfacial deposition and the local structure of transition metal ioni251
  • 1. Introduction251
  • 2. Experimental methodologies for investigating the mode of interfacial deposition and the local str254
  • Acknowledgment258
  • References258
  • Synthesis and characterization of nanocrystal zeolite/mesoporous matrix composite material259
  • 1. Introduction259
  • 2. Experimental section260
  • 3. Results and discussions261
  • 4. Conclusion266
  • 5. Acknowledgments266
  • References266
  • On the role of iron in preparation of mesoporous Fe-MFI zeolites via desilication267
  • Abstract267
  • 1. Introduction267
  • 2. Experimental268
  • 3. Results and discussion269
  • 4. Conclusions274
  • References274
  • Selective formation of p-xylene over single crystal-like zeolite composite275
  • 1. Introduction275
  • 2. Experimental section276
  • 3. Results and discussion277
  • 4. Conclusions281
  • Acknowledgements282
  • References282
  • Control of the basic sites strength by adjusting the active species dispersion283
  • 1. Introduction283
  • 2. Experimental part284
  • 3. Results286
  • 4. Conclusions290
  • References290
  • A new approach of hydrotreating catalysts preparation by support functionalization291
  • 1. Introduction291
  • 2. Experimental293
  • 3. Results294
  • 4. Discussion297
  • 5. Conclusion297
  • Acknowledgements298
  • References298
  • Preparation, characterization and catalytic performances of highly dispersed supported TiO2/SiO2 cat299
  • Abstract299
  • 1. Introduction299
  • 2. Experimental300
  • 3. Results and discussion301
  • 4. Conclusion305
  • Aknowledgements306
  • References306
  • New synthesis method for metal phosphide hydrotreating catalysts: MoP/SiO2 and MoP/AI2O3307
  • Abstract307
  • 1. Introduction307
  • 2. Experimental307
  • 3. Results and discussion308
  • 4. Conclusions314
  • References314
  • Structural and catalytic properties of amorphous mesoporous AIPO4 materials prepared in the presence315
  • 1. Introduction315
  • 2. Experimental316
  • 3. Results and discussion316
  • 4. Conclusions322
  • Acknowledgment322
  • References322
  • Mesoporous ZSM-5 synthesized by simultaneous mesostructuring and crystallisation of ZSM-5 nuclei323
  • 1. Introduction323
  • 2. Experimental324
  • 3. Results325
  • 4. Discussion329
  • 5. Conclusion329
  • Acknowledgements330
  • References330
  • Preparation of new type of CaSiO3 with high surface area and property as a catalyst support331
  • Abstract331
  • 1. Introduction331
  • 2. Experimental332
  • 3. Results and Discussion333
  • 4. Conclusion338
  • Reference338
  • On the role of organic amine templates in the synthesis of AlPO molecular sieves: An experimental an339
  • Abstract339
  • 1. Introduction339
  • 2. Computational methods and experimental syntheses340
  • 3. Results and discussion341
  • 4. Conclusions346
  • Acknowledgments346
  • References346
  • Secondary crystallisation of SBA-15 in the presence of TPAOH and aqueous glycerol - Influence of the347
  • 1. Introduction347
  • 2. Experimental348
  • 3. Results349
  • 4. Discussion352
  • 5. Conclusion354
  • Acknowledgements354
  • References354
  • New NiMo catalysts supported on ZrO2-modified SBA-15 materials for 4,6-dimethyldibenzothiophene hydr355
  • 1. Introduction355
  • 2. Experimental356
  • 3. Results and Discussion356
  • 4. Conclusions362
  • Acknowledgements362
  • References362
  • Textural and redox properties of CeO2 nanoparticles prepared by using a non-ionic surfactant363
  • 1. Introduction363
  • 2. Experimental Procedure364
  • 3. Results and discussion364
  • References368
  • Acknowledgements368
  • Preparation of SnO2 nanocrystallites-incorporated large mesoporous silica materials in self-generate369
  • 1. Introduction369
  • 2. Materials and methods370
  • 3. Results and discussion371
  • 4. Conclusions375
  • Acknowledgements376
  • References376
  • Preparation of stable mesoporous titanium oxides nanomaterials using soluble starch377
  • Abstract377
  • 1. Introduction377
  • 2. Experimental378
  • 3. Results and discussions379
  • 4. Conclusion and prospects383
  • Acknowledgements384
  • References384
  • Novel mesoporous cerium oxide for air purification material385
  • 1. Introduction385
  • 2. Experimental386
  • 3. Results and Discussions387
  • 4. Conclusions390
  • References390
  • Size and shape control of gamma-AIOOH boehmite nanoparticles, a precursor of gamma-AI2O3 catalyst393
  • 1. Introduction393
  • 2. Experimental394
  • 3. Results and discussion395
  • 4. Conclusion399
  • Acknowledgements399
  • References400
  • Synthesis of Pt- modified MCM-41 mesoporous molecular sieve catalysts: Influence of methods of Pt in401
  • 1. Introduction401
  • 2. Experimental402
  • 3. Results and discussion404
  • 4. Conclusions407
  • Acknowledgements408
  • References408
  • Mesoporous ZSM-5 prepared by sequential nano-casting of MCM-41 nanospheres409
  • 1. Introduction409
  • 2. Experimental410
  • 3. Results411
  • 4. Discussion415
  • 5. Conclusion416
  • Acknowledgements416
  • References416
  • Noncovalent anchoring of hydride tungsten complex on mesoporous materials417
  • 1. Introduction417
  • 2. Experimental418
  • 3. Results and Discussion420
  • 4. Conclusions423
  • Acknowledgments424
  • References424
  • Facile preparation of nanostructured manganese oxides by hydrotreatment of commercial particles425
  • 1. Introduction425
  • 2. Experimental426
  • 3. Results and Discussion427
  • 4. Conclusions431
  • Acknowledgements432
  • References432
  • Mordenite seeding gels mesostructured by the non-ionic surfactant Pluronic P123433
  • 1. Introduction433
  • 2. Experimental433
  • 3. Results435
  • 4. Discussion439
  • 5. Conclusion440
  • Acknowledgements440
  • References440
  • Synthesis and surface reactivity of nanocomposite support Al2O3/alpha-AI2O3441
  • 1. Introduction441
  • 2. Experimental442
  • 3. Results and discussion444
  • 4. Conclusion448
  • Reference448
  • Preparation of Pt°/MCM-41: effect of drying on MCM-41 structure and Pt° dispersion449
  • 1. Abstract449
  • 2. Introduction449
  • 3. Experimental450
  • 4. Results451
  • 5. Discussion454
  • 6. Conclusion456
  • 7. Acknowledgments456
  • References456
  • Ag-CsOH/SiO2 bi-functional catalysts for production of methyl methacrylate from methyl propionate an457
  • 1. Introduction457
  • 2. Catalysts for aldol-type-condensation reaction458
  • 3. Characteristics of Ag-CsOH/SiO2 catalys459
  • 4. Oxidation of Methanol to HCHO in the presence of MP460
  • 5. Performances of combined catalyst system462
  • 6. Conversion of methanol in the absence of MP463
  • 7. Conclusion464
  • References464
  • Optimized conditions for the preparation of Pt supported catalysts by deposition-precipitation465
  • Abstract465
  • 1. Introduction465
  • 2. Experimental466
  • 3. Results and discussion468
  • 4. Conclusions471
  • Acknowledgements472
  • References472
  • Controlled synthesis of supported ruthenium catalysts for CO oxidation by organometallic chemical va473
  • Abstract473
  • 1. Introduction473
  • 2. Experimental474
  • 3. Results and Discussion475
  • 4. Conclusions480
  • Acknowledgement480
  • References480
  • PdGa and Pd3Ga7: highly-selective catalysts for the acetylene partial hydrogenation481
  • Abstract481
  • 1. Introduction481
  • 2. Experimental482
  • 3. Results and Discussion483
  • 4. Conclusions487
  • Acknowledgement488
  • References488
  • Preparation and properties of Pt-Mo sulfide system supported on mesoporous silica-alumina489
  • 1. Introduction489
  • 2. Experimental490
  • 3. Results and discussion491
  • 4. Conclusions496
  • Acknowledgement496
  • References496
  • Modification method studies for the preparation of tartaric acid-NaBr-modified nickel catalyst for t497
  • 1. Introduction497
  • 2. Experimental498
  • 3. Results and Discussion500
  • 4. Conclusion503
  • Acknowledgments504
  • References504
  • Preparation of noble metal catalysts by atomic layer deposition: FTIR studies505
  • Abstract505
  • 1. Introduction505
  • 2. Experimental506
  • 3. Results and discusston507
  • 4. Conclusions511
  • Acknowledgements512
  • References512
  • Platinum nanoparticles incorporated in mesoporous silica SBA-15 by the deposition-precipitation meth513
  • Abstract513
  • 1. Introduction513
  • 2. Experimental514
  • 3. Results and discussion515
  • 4. Conclusion519
  • Acknowledgment520
  • References520
  • Immobilizing metal nanoparticles in porous silica through sol-gel process521
  • 1. Introduction521
  • 2. Experimental522
  • 3. Results524
  • 4. Discussion527
  • 5. Conclusions528
  • Acknowledgements528
  • References528
  • Pt/SiO2 catalyst preparation: high platinum dispersions by using low-temperature treatments529
  • Abstract529
  • 1. Introduction529
  • 2. Experimental530
  • 3. Results531
  • 4. Discussion534
  • 5. Conclusions536
  • Acknowledgements536
  • References536
  • Preparation of ultra high loading supported Pt catalyst for direct methanol fuel cell537
  • 1. Introduction537
  • 2. Experimental538
  • 3. Results and discussion540
  • 4. Conclusion544
  • References544
  • Towards more gold and less chlorine on the support during the deposition-precipitation of gold545
  • Abstract545
  • 1. Introduction545
  • 2. Experimental546
  • 3. Results and Discussion547
  • 4. Conclusions551
  • Acknowledgements552
  • References552
  • Single-phase bimetallic system for the selective oxidation of glycerol to glycerate553
  • Abstract553
  • 1.Introduction553
  • 2.Experimental554
  • 3.Results and discussion555
  • 1. Conclusions559
  • References559
  • Surfactant-mediated synthesis of Pt nanoparticles/nanoporous carbons composite561
  • 1. Introduction561
  • 2. Experimental562
  • 3. Results and discussion563
  • 4. Conclusions567
  • Acknowledgments567
  • References567
  • Grafting of coordination compounds onto functionalized carbon supports as precursors for bimetallic569
  • Abstract569
  • 1. Introduction569
  • 2. Experimental571
  • 3. Results and discussion572
  • 4. Conclusion576
  • Acknowledgements576
  • References576
  • Well-defined Rh/AI2O3 catalysts selectively poisoned by Ge: A new tool to study reaction pathways577
  • Abstract577
  • 1. Introduction577
  • 2. Experimental578
  • 3. Results and discussion580
  • 4. Conclusion583
  • References584
  • Specific performance of silica-coated Pt catalyst for the competitive combustion of methane and othe585
  • 1. Introduction585
  • 2. Experimental586
  • 3. Results and discussion587
  • 4. Conclusion592
  • References592
  • Influence of the Ti precursor used for the grafting of SiO2 on the catalytic properties of Rh/Ti-SiO593
  • Abstract593
  • 1. Introduction593
  • 2. Experimental594
  • 3. Results595
  • 4. Discussion598
  • 5. Conclusion600
  • Acknowledgements600
  • References600
  • Preparation of PD on carbon black by deposition-precipitation: Study of the effect of the support fu601
  • Abstract601
  • 1. Introduction601
  • 2. Material and methods602
  • 3. Results604
  • 4. Discussion607
  • 5. Conclusions608
  • Acknowledgment608
  • References608
  • Preparation of ruthenium supported catalysts for wet air oxidation of p-hydroxybenzoic acid609
  • Abstract609
  • 1. Introduction609
  • 2. Experimental610
  • 3. Results and discussion612
  • 4. Conclusion616
  • Acknowledgements616
  • References616
  • PtSn/C electrocatalysts prepared by different methods for direct ethanol fuel cell617
  • 1. Introduction617
  • 2. Experimental618
  • 3. Results and discussion619
  • 4. Conclusions623
  • Acknowledgments623
  • References623
  • Gas phase synthesis of metal oxide monolithic catalysts for hydrocarbon deep oxidation625
  • Abstract625
  • 1. Introduction625
  • 2. Experimental626
  • 3. Results and Discussion628
  • 4. Conclusions631
  • References632
  • Ni thin layer catalysts for making H2 "COx free" by decomposition of natural gas in a structured mul633
  • Abstract633
  • 1. Introduction634
  • 2. Experimental634
  • 3. Results and Discussion636
  • 4. Conclusions640
  • 5. References640
  • CrAI alloy-based cermet monolith with polymodal pore structure for partial oxidation of methane to s641
  • 1. Introduction641
  • 2. Experimental642
  • 3. Results and Discussion643
  • Conclusions648
  • Acknowledgments648
  • References648
  • Ceramic catalysts for the decomposition of H2O2 - Influence of wash-coat procedure and active phase649
  • Abstract649
  • 1. Introduction649
  • 2. Experimental part651
  • 3. Results652
  • 4. Conclusions656
  • Acknowledgments656
  • References656
  • Supported Co3O4-CeO2 monoliths: effect of preparation method and Pd-Pt promotion on the CO/CH4 oxida657
  • Abstract657
  • Introduction658
  • Experimental659
  • Results and discussion660
  • Conclusions664
  • References664
  • Preparation of metal supported hexaaluminate catalyst for methane combustion665
  • Abstract665
  • 1. Introduction665
  • 2. Experimental666
  • 3. Results667
  • 4. Discussion670
  • 5. Conclusions671
  • Acknowledgement672
  • References672
  • Bifunctional catalytic PVA composites for the one pot synthesis of camphor from camphene673
  • Abstract673
  • 1. Introduction673
  • 2 Experimental674
  • 3. Results and discussion676
  • 4. Conclusions680
  • References680
  • Structured Pd/gamma-AI2O3 catalysts on FeCrAlloy fibers for total combustion of methane681
  • Abstract681
  • 1. Introduction681
  • 2. Experimental682
  • 3. Results and Discussion684
  • 4. Conclusions687
  • Acknowledgements687
  • References688
  • Preparation in mild conditions of photocatalytically active nanostructured TiO2 rutile689
  • Abstract689
  • 1. Introduction689
  • 2. Experimental690
  • 3. Results and Discussion691
  • 4. Conclusion696
  • References696
  • Supported vanadium oxide nanoparticles: effect of preparation method, support and type of precursor697
  • Abstract697
  • 1. Introduction697
  • 2. Experimental698
  • 3. Results and discussion699
  • 4. Conclusions703
  • Aknowledgement704
  • References704
  • Microwaves-assisted synthesis of La1-x AgxMnO3+delta (0 ≤ x ≤ 0.2) perovskites with high surfa705
  • Abstract705
  • 1. Introduction705
  • 2. Experimental706
  • 3. Results708
  • 4. Conclusions712
  • Acknowledgements712
  • References712
  • Origin of the dispersion limit in the preparation of Ni(Co)Mo/AI2O3 and Ni(Co)Mo/TiO2 HDS oxidic pre713
  • 1. Introduction713
  • 2. Experimental714
  • 3. Results and Discussion715
  • 4. Conclusion719
  • References720
  • Preparation of Pd/C catalysts: from the Pd-precursor solution to the final systems721
  • 1. Introduction721
  • 2. Experimental722
  • 3. Characterization of the supports722
  • 4. Pd precipitation from Na2PdCl4 solution723
  • 5. Catalyst preparation726
  • Acknowledgments728
  • Refrences728
  • Large-scale synthesis and forming of xerogel catalysts729
  • 1. Introduction729
  • 2. Experimental730
  • 3. Results and discussion732
  • 4. Conclusions736
  • Acknowledgement736
  • References736
  • Preparation of Co3O4 catalysts for direct decomposition of nitrous oxide under industrial conditions737
  • Abstract737
  • 1. Introduction737
  • 2. Experimental738
  • 3. Results and discussion739
  • 4. Conclusions744
  • References744
  • Spin-coating of mixed citrate complexes as a versatile route to prepare films of transition metal mu745
  • Abstract745
  • 1. Introduction745
  • 2. Experimental747
  • 3. Results and discussion748
  • 4. Conclusions751
  • Acknowledgements752
  • References752
  • The influence of the preparation method on the catalytic properties of lanthanum-doped hematite in t753
  • 1. Introduction753
  • 2. Experimental754
  • 3. Results and Discussion755
  • 4. Conclusions760
  • 5. References760
  • Microwave-assisted catalysts for the CPO of methane761
  • 1. Introduction761
  • 2. Experimental762
  • 3. Results and Discussion763
  • 4. Conclusions768
  • Acknowlegements768
  • References768
  • Preparation of Mo-V-Te-Nb mixed oxides using the template route769
  • Abstract769
  • 1. Introduction769
  • 2. Experimental770
  • 3. Results and discussion771
  • 4. Conclusion776
  • Acknowledgements776
  • References776
  • Preparation of CeO2/ZrO2 modified by MgO: Roles of MgO for upgrading redox property777
  • 1. Abstract777
  • 2. Introduction777
  • 3. Experimental778
  • 4. Results and Discussion779
  • 5. References784
  • Preparation of V2O5/TiO2 catalyst for NH3-SCR: Controlling factor of TiO2 support for highly active785
  • Abstract785
  • 1. Introduction785
  • 2. Experimental786
  • 3. Results787
  • 4. Discussion790
  • References792
  • Polymer-immobilized aluminium or copper tungstophosphates and tungstosilicates as new catalysts in t793
  • Abstract793
  • 1. Introduction793
  • 2. Experimental794
  • 3. Results and discussion795
  • Acknowledgements800
  • References800
  • Preparation of heteropolyacid/carbon catalyst and its application to methacrolein oxidation801
  • Abstract801
  • 1. Introduction801
  • 2. Experimental802
  • 3. Results and discussion803
  • 4. Conclusions807
  • Acknowledgements808
  • References808
  • Towards the local structure of the Co(ll), Ni(ll), Cr(VI) and W(VI) ionic species formed upon impreg809
  • Abstract809
  • 1. Introduction809
  • 2. Experimental810
  • 3. Results and Discussion810
  • Conclusions816
  • Acknowledgment816
  • References816
  • Urea-matrix combustion method: a versatile tool for the preparation of HDS catalysts817
  • 1. Introduction817
  • 2. Experimental818
  • 3. Results and discussion819
  • 4. Conclusions823
  • Acknowledgment824
  • 5. References824
  • Catalytic properties of strontium ruthenate perovskite prepared by hot isostatic pressure method825
  • 1. Abstract825
  • 2. Introduction826
  • 3. Experimental827
  • 4. Results and Discussion828
  • 5. Conclusion830
  • 6. Acknowledgements830
  • References831
  • Effect of the particle size and the active phase composition in CoFe/gammaAl2O3 catalyst on the mult833
  • Abstract833
  • 1. Introduction833
  • 2. Experimental834
  • 3. Results and discussion835
  • 4. Conclusions840
  • Acknowledgements840
  • References840
  • Sol-Gel synthesis and characterizaion of Nb-Mo and Nb-Mo-V mixed oxides as potential catalysts for t841
  • Abstract841
  • 1. Introduction841
  • 2. Experimental842
  • 3. Results and Discussion843
  • 4. Conclusions847
  • References848
  • Structure control of molybdenum sulfide clusters encaged in zeolite prepared by a CVD technique849
  • Abstract849
  • 1. Introduction849
  • 2. Experimental850
  • 3. Results and Discussion852
  • 4. Conclusions856
  • 5. References856
  • Nitridation of ultrastable Y zeolite: influence of the experimental parameters857
  • Abstract857
  • 1. Introduction857
  • 2. Experimental858
  • 3. Results and discussion859
  • 4. Conclusion864
  • Acknowledgements864
  • References864
  • An investigation into the use of seeding in the vapour phase synthesis of self-supporting zeolite ZS865
  • 1. Introduction865
  • 2. Experiments866
  • 3. Results and discussion868
  • 4. Conclusion871
  • 5. Acknowledgements872
  • References872
  • Synthesis of MTT zeolite catalysts with surface Al depletion873
  • 1. Introduction874
  • 2. Experimental874
  • 3. Results and discussion875
  • 4. Conclusions880
  • Acknowledgments880
  • References880
  • Synthesis of zeolite ZSM-35 bulk material from aluminosilicate amorphous sinter881
  • 1. Introduction881
  • 2. Experiments882
  • 3. Results and discussion883
  • 4. Conclusion887
  • 5. Acknowledgements888
  • Reference888
  • Targeted preparation of Fe-zeolites with iron prevailing in extraframework cationic positions889
  • 1. Introduction889
  • 2. Experimental891
  • 3. Results and discussion892
  • 4. Conclusions896
  • Acknowledgements896
  • References896
  • Preparation factors influencing the effectiveness of SAPO catalysts in n-paraffins hydroisomerizatio897
  • 1. Introduction897
  • 2. Experimental898
  • 3. Results and discussion899
  • 4. Conclusion904
  • 5. References904
  • Formation of mesopores in ZSM-5 by carbon templating905
  • 1. Introduction905
  • 2. Experimental906
  • 3. Results and discussion908
  • 4. Conclusions911
  • Acknowledgements912
  • References912
  • Catalysts for non-oxidative methane conversion913
  • Abstract913
  • 1. Introduction913
  • 2. Experimental914
  • 3. Results and discussion915
  • 4. Conclusions920
  • References920
  • Effect of nitridation on the selectivity of (gallo) alumino-phosphates for mixed aldol condensation921
  • 1. Introduction921
  • 2. Experimental922
  • 3. Results and discussion924
  • 4. Conclusions928
  • Acknowledgements928
  • References928
  • Preparation and utilization of CaF2-Zr02 as a novel solid base for the synthesis of dimethyl carbona929
  • Abstract929
  • 1. Introduction929
  • 2. Experimental930
  • 3. Results and discussions931
  • 4. Conclusions935
  • Reference936
  • Pd/AI18B4O33: Synthesis and application in the high temperature catalytic combustion of methane937
  • Abstract937
  • 1. Introduction937
  • 2. Experimental938
  • 3. Results and discussion939
  • 4. Conclusions943
  • Acknowledgements943
  • References943
  • Effect of Fe or Cu addition on Ni/Mg-AI and Ni/MgO catalysts in the steam-reforming of methane945
  • 1. Introduction946
  • 2. Experimental946
  • 3. Results and discussion947
  • 4. Conclusion952
  • 5. Acknowledgement952
  • 6. References952
  • Comparative study of the sulfur loss in the xerogel and aerogel sulfated zirconia calcined at differ953
  • Abstract953
  • 1. Introduction953
  • 2. Experimental954
  • 3. Results and discussion955
  • 4. Conclusion960
  • Acknowledgement960
  • References960
  • Preparation of isolated highly dispersed titanium oxides on silica by sol-gel method for photocataly961
  • 1. Introduction961
  • 2. Experimental962
  • 3. Results and discussion963
  • 4. Conclusions967
  • Acknowledgements968
  • References968
  • Shape forming of Pt/AI2O3Si sol-gel catalysts for space applications969
  • 1. Introduction969
  • 2. Experimental970
  • 3. Results972
  • 4. Conclusions976
  • References976
  • A new citrate route for the synthesis of catalysts easy to scale-up and environmentally friendly977
  • Abstract977
  • 1. Introduction977
  • 2. Experimental979
  • 3. Results and discussion979
  • 4. Conclusions983
  • References984
  • Acknowledgments984
  • Preparation of low temperature water-gas shift catalysts by flame spray pyrolysis985
  • 1. Abstract985
  • 2. Introduction985
  • 3. Experimental986
  • 4. Results and discussion987
  • 5. Conclusions991
  • 6. Acknowledgements992
  • References992
  • Preparation of transition metal fluorides as catalysts for the environmentally sustainable HFC produ993
  • 1. Introduction993
  • 2. Experimental994
  • 3. Results and Discussion994
  • 4. Conclusions999
  • Acknowledgements1000
  • 5. Bibliography1000
  • Preparation of alkali-earth tantalum oxynitride photocatalyst worked under visible light utilized by1001
  • 1. Introduction1001
  • 2. Experimental1002
  • 3. Results and Discussion1003
  • 4. Conclusion1007
  • Acknowledgments1008
  • References1008
  • Alternative supports for the catalysts preparation for low-temperature fuel cells using the Alcohol1009
  • Abstract1009
  • 1. Introduction1009
  • 2. Experimental1010
  • 3. Results and Discussion1011
  • 4. Conclusion1015
  • Acknowledgments1016
  • References1016
  • Gold catalysts supported on mixed oxides for hydrogen production1017
  • 1. Introduction1018
  • 2. Experimental1018
  • 3. Results and discussion1020
  • 4. Conclusions1023
  • Acknowledgements1024
  • References1024
  • Highly dispersed cerium and titanium oxides on silica prepared by impregnation method for photocatal1025
  • 1. Introduction1025
  • 2. Experimental1026
  • 3. Results and discussion1027
  • 4. Conclusions1032
  • Acknowledgements1032
  • References1032
  • Authors index1033
  • Studies in Surface Science and Catalysis1039
Book details
  • Vendor Elsevier S & T
  • SKU 9780444528278
  • ISBN-13 9780080467245
  • Author Gaigneaux*, E.; Devillers, M; De Vos**, D.E.; Hermans, S.; Jacobs, P.; Martens, J.; Ruiz, P.
  • Category Science
  • Subject Physical & Theoretical

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This volume of Studies in Surface Science and Catalysis contains the Proceedings of the 9th International Symposium on the Scientific Bases for the Preparation of Heterogeneous Catalysts, held on the campus of the "Universit catholique de Louvain" (UCL) in Louvain-la-Neuve, Belgium, on September 10-14, 2006. This series of symposia was initiated in 1975 on a regular 4-year interval basis.
The Symposium covered the following topics: key aspects in catalysts preparation, micro- and mesoporous supports, supported metal catalysts, structured catalysts, tailored zeolites, catalysis by bases, and catalysts for fuel production. These topics served as guidelines for the sessions both in the programs of oral communications (41 contributions including 7 keynote communications – one for each topic) and poster presentations (101 contributions). In addition, the opening invited lecture addressed the question of scaling-up high-throughput experimental approaches.

* Contains a collection of the papers presented at the workshop