Elsevier S & T

Solving Problems with NMR Spectroscopy

Atta-ur-Rahman; Choudhary, Muhammad Iqbal

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Table of contents
  • Solving Problems with NMR Spectroscopyi
  • Copyright Pageii
  • Contentsv
  • Forewordxi
  • Forewordxiii
  • Prefacexv
  • Chapter 1. The Basics of Modern NMR Spectroscopy1
  • 1.1 WHAT IS NMR?1
  • 1.2 INSTRUMENTATION9
  • 1.3 CREATING NMR SIGNALS20
  • SOLUTIONS TO PROBLEMS74
  • REFERENCES89
  • Chapter 2. Spin-Echo and Polarization Transfer91
  • 2.1 SPIN-ECHO FORMATION IN HOMONUCLEAR AND HETERONUCLEAR SYSTEMS91
  • 2.2 CROSS-POLARIZATION103
  • 2.3 POLARIZATION TRANSFER IN REVERSE121
  • SOLUTIONS TO PROBLEMS131
  • REFERENCES146
  • Chapter 3. The Second Dimension149
  • 3.1 DATA ACQUISITION IN 2D NMR156
  • 3.2 DATA PROCESSING IN 2D NMR163
  • 3.3 PLOTFING OF 2D SPECTRA175
  • SOLUTIONS TO PROBLEMS175
  • REFERENCES185
  • Chapter 4. Nuclear Overhauser Effect187
  • 4.1 nOe AND SELECTIVE POPULATION TRANSFER188
  • 4.2 RELAXATION189
  • 4.3 MECHANISM OF nOe190
  • 4.4 FACTORS AFFECTING nOe195
  • 4.5 SOME PRACTICAL HINTS204
  • SOLUTIONS TO PROBLEMS207
  • REFEREN CES211
  • Chapter 5. Important 2D NMR Experiments213
  • 5.1 HOMO- AND HETERONUCLEAR J-RESOLVED SPECTROSCOPY213
  • 5.2 HOMONUCLEAR AND HETERONUCLEAR SHIFT- CORRELATION SPECTROSCOPY235
  • 5.3 TWO-DIMENSIONAL NUCLEAR OVERHAUSER SPECTROSCOPY259
  • 5.4 TWO-DIMENSIONAL CHEMICAL EXCHANGE SPECTROSCOPY265
  • 5.5 HOMONUCLEAR HARTMANN-HAHN SPECTROSCOPY (HOHAHA), OR TOTAL CORRELATION SPECTROSCOPY (TOCSY)267
  • 5.6 "INVERSE" NMR SPECTROSCOPY271
  • 5.7 INADEQUATE274
  • SOLUTIONS TO PROBLEMS305
  • REFERENCES343
  • Chapter 6. The Third Dimension345
  • 6.1 BASIC PHILOSOPHY345
  • 6.2 TYPES AND POSITIONS OF PEAKS IN 3D SPECTRA348
  • REFERENCES362
  • Chapter 7. Recent Developments in NMR Spectroscopy365
  • 7.1 SELECTIVE PULSES IN MODERN NMR SPECTROSCOPY365
  • 7.2 ONE-DIMENSIONAL EXPERIMENTS USING SOFT PULSES366
  • 7.3 HETERONUCLEAR SELECTIVE 1D NMR EXPERIMENTS371
  • 7.4 TWO-DIMENSIONAL EXPERIMENTS USING SOFT PULSES373
  • 7.5 SOFT EXCITATION IN TWO DIMENSIONS377
  • 7.6 THREE-DIMENSIONAL EXPERIMENTS USING SOFT PULSES380
  • 7.7 FIELD GRADIENTS381
  • REFERENCES389
  • Chapter 8. Logical Protocols for Solving Complex Structural Problems391
  • 8.1 3-HYDROXYLUPANINE (1)394
  • 8.2 (+)-BUXALONGIFOLAMIDINE (2)398
  • REFERENCES409
  • GLOSSARY411
  • Index421
Book details
  • Vendor Elsevier S & T
  • SKU 9780120663200
  • ISBN-13 9780080541495
  • Author Atta-ur-Rahman; Choudhary, Muhammad Iqbal
  • Category Science
  • Subject Analytic

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Solving Problems with NMR Spectroscopy presents the basic principles and applications of NMR spectroscopy with only as much math as is necessary. It shows how to solve chemical structures with NMR by giving clear examples and solutions. This text will enable organic chemistry students to choose the most appropriate NMR techniques to solve specific structures. The problems to work and the discussion of their solutions and interpretations will help readers becomeproficient in the application of important, modern 1D and 2D NMR techniques to structural studies.

Key Features
* Presents the most important NMR techniques for structural determinations
* Offers a unique problem-solving approach
* Uses questions and problems, including discussions of their solutions and interpretations, to help readers grasp NMR
* Avoids extensive mathematical formulas
* Forewords by Nobel Prize winner Richard R. Ernst and Lloyd M. Jackman