Elsevier S & T

Verified Synthesis of Zeolitic Materials: Second Edition

Robson, H.

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Table of contents
  • Cover
  • Table of contentsv
  • Preface1
  • Synthesis commission: membership2
  • Introduction and explanatory notes3
  • Conditions for recording of XRD patterns7
  • Contributors8
  • Part I: Introduction to zeolite synthesis19
  • Chapter 1. Source materials for zeolite synthesis19
  • Chapter 2. Nucleation. growth. and seeding in zeolite synthesis21
  • Chapter 3. Synthesis of high-silica zeolites and phosphate-based materials in the presence of fluori25
  • Chapter 4. Templating in molecular sieve synthesis27
  • Chapter 5. The pH value and its importance for the crystallization of zeolites33
  • Chapter 6. Microwave technology in zeolite synthesis39
  • Chapter 7. Preparation of zeolite membranes43
  • Chapter 8. Safety considerations for zeolite synthesis45
  • Chapter 9. Product characterization by x-ray powder diffraction47
  • Chapter 10. Determination of the elemental compositor of zeolitic materials51
  • Chapter 11.Characterization of zeolites by SEM55
  • Chapter 12. Product characterization by NMR57
  • Chapter 13. Characterization of zeolites by sorption capacity measurements61
  • Chapter 14. Ion-exchange capacity67
  • Chapter 15. Characterization by IR spectroscopy69
  • Chapter 16. How to read a patent73
  • Part II: Synthesis recipes74
  • Chapter 17. ABW - Li-A (BW)74
  • Chapter 18. AEI - AlPO4-1878
  • Chapter 19. AEI - SAPO-18 (DPEA method)81
  • Chapter 20. AEI - SAPO-18 (TEA method)84
  • Chapter 21. AEL - AlPO4-1187
  • Chapter 22. AFI - AlPO4-590
  • Chapter 23. AFI - SAPO-593
  • Chapter 24. AFI - COAPO-596
  • Chapter 25. AFI - SSZ-2499
  • Chapter 26. AFO - SAPO-41102
  • Chapter 27. AFS - MAPO-46105
  • Chapter 28. ANA - Analcime107
  • Chapter 29. AST - AlPO4-16110
  • Chapter 30. ATN - MAPO-39113
  • Chapter 31. BEA - Zeolite Beta115
  • Chapter 32. BEA - [Ti, Al] Beta118
  • Chapter 33. CAN - Cancrinite121
  • Chapter 34. CHA - Chabazite123
  • Chapter 35. CHA - SSZ-13126
  • Chapter 36. CHA - SAPO-34129
  • Chapter 37. CHA - SAPO-44132
  • Chapter 38. -CLO - Cloverite (GaPO4)134
  • Chapter 39. EAB - TMA-E137
  • Chapter 40. EDI - Barrer K-F140
  • Chapter 41. EDI - Linde Type F142
  • Chapter 42. EMT - EMC-2145
  • Chapter 43. EUO - [Ga] EU-1147
  • Chapter 44. FAU - Linde Type X150
  • Chapter 45. FAU - Low-silica Type X ( LSX )153
  • Chapter 46. FAU - Linde Type Y156
  • Chapter 47. FAU - High-silica Faujasite EMC-1159
  • Chapter 48. FAU - [Ga] Type Y162
  • Chapter 49. FAU - SAPO-37164
  • Chapter 50. FER - ZSM-3 5167
  • Chapter 51. GIS - Zeolite P169
  • Chapter 52. KFI - ZK-5171
  • Chapter 53. KFI - High-silica KFI174
  • Chapter 54. LEV - [B]-Levyne177
  • Chapter 55. LTA - Linde Type A179
  • Chapter 56. LTA - ZK-4182
  • Chapter 57. LTA - Zeolite Alpha185
  • Chapter 58. LTA - GaPO4188
  • Chapter 59. LTL - Linde Type L190
  • Chapter 60. MAZ - Mazzite193
  • Chapter 61. MER - Linde W196
  • Chapter 62. MFI - High-alumina ZSM-5198
  • Chapter 63. MFI - Silicalite-l201
  • Chapter 64. MFI - [B] ZSM-5203
  • Chapter 65. MFI - [Fe] ZSM-5205
  • Chapter 66. MFI - [Ti] ZSM-5207
  • Chapter 67. MFI - [Ti, Al] ZSM-5209
  • Chapter 68. MOR - Mordenite212
  • Chapter 69. MTN - ZSM-39214
  • Chapter 70. MTT - ZSM-23217
  • Chapter 71. MTW - ZSM-12220
  • Chapter 72. MTW- [Ga] ZSM-12222
  • Chapter 73. MWW - MCM-22225
  • Chapter 74. NAT - [Ga] Natrolite228
  • Chapter 75. OFF - Linde Type T230
  • Chapter 76.OFF - Offretite233
  • Chapter 77. OFF - [Ga] Offretite236
  • Chapter 78. PAU - ECR-18239
  • Chapter 79. PAU - Paulingite (seeded)241
  • Chapter 80. PHI - Phillipsite244
  • Chapter 81. PHI - High-alumina Phillipsite246
  • Chapter 82. RHO - High-silica Rho249
  • Chapter 83. SOD - NaBr-Sodalite251
  • Chapter 84. STT - SSZ-23255
  • Chapter 85. TON - ZSM-22258
  • Chapter 86. VFI - VPI-5 (DPA method)261
  • Chapter 87. VFI - VPI-5 (TBA method)263
  • Chapter 88. -SUZ-4265
Book details
  • Vendor Elsevier S & T
  • SKU 9780444507037
  • ISBN-13 9780080543512
  • Author Robson, H.
  • Edition 2nd
  • Category Architecture
  • Subject Methods & Materials

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Zeolite synthesis is an active field of research. As long as this continues, new phases will be discovered and new techniques for preparing existing phases will appear. This edition of Verified Synthesis of Zeolitic Materials contains all the recipes from the first edition plus 24 new recipes. Five new introductory articles have been included plus those from the first edition, some of which have been substantially revised. The XRD patterns have been recorded using different instrument settings from those in the first edition and are intended to conform to typical X-ray diffraction practice. In most cases, only the XRD pattern for the productas synthesised is printed here. The exceptions are those phases which show marked changes in the XRD pattern upon calcination.